N-benzoyl-4-chloro-2-cyanobutanamide

Base Information

Chemical Name:N-benzoyl-4-chloro-2-cyanobutanamide
CAS No.:133036-73-4
Molecular Formula:C₁₂H₁₁ClN₂O₂
Molecular Weight:250.685
Hs Code.:

Synonyms:N-benzoyl-4-chloro-2-cyanobutanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-benzoyl-4-chloro-2-cyanobutanamide

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Technology Process of N-benzoyl-4-chloro-2-cyanobutanamide

There total 3 articles about N-benzoyl-4-chloro-2-cyanobutanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 133036-74-5
N-benzoyl-1-cyanocyclopropanecarboxamide

: 133036-73-4
N-benzoyl-4-chloro-2-cyanobutanamide

Guidance literature:: With titanium tetrachloride; In chloroform; for 1h; Heating;

Reference yield: 82.0%

: 98061-56-4
2-benzamido-4,5-dihydro-3-furancarbonitrile

: 133036-73-4
N-benzoyl-4-chloro-2-cyanobutanamide

Guidance literature:: With titanium tetrachloride; In chloroform; for 1h; Product distribution; Mechanism; Heating; other 2-acylamino-4,5-dihydro-3-furancarbonitriles;

Reference yield:

: 91036-81-6
N-benzoyl-α-cyanoacetamide

: 133036-73-4
N-benzoyl-4-chloro-2-cyanobutanamide

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) 60percent NaH / 1.) DMF, RT, 2.) RT, 30 min

2: 89 percent / TiCl₄ / CHCl₃ / 1 h / Heating

With titanium tetrachloride; sodium hydride; In chloroform;