[3-Bromo-4-(3-diethylamino-propoxy)-phenyl]-(1-bromo-2-ethyl-indolizin-3-yl)-methanone

Base Information

Chemical Name:[3-Bromo-4-(3-diethylamino-propoxy)-phenyl]-(1-bromo-2-ethyl-indolizin-3-yl)-methanone
CAS No.:79286-30-9
Molecular Formula:C₂₄H₂₈Br₂N₂O₂
Molecular Weight:536.307
Hs Code.:

Synonyms:[3-Bromo-4-(3-diethylamino-propoxy)-phenyl]-(1-bromo-2-ethyl-indolizin-3-yl)-methanone

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Chemical Property of [3-Bromo-4-(3-diethylamino-propoxy)-phenyl]-(1-bromo-2-ethyl-indolizin-3-yl)-methanone

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Technology Process of [3-Bromo-4-(3-diethylamino-propoxy)-phenyl]-(1-bromo-2-ethyl-indolizin-3-yl)-methanone

There total 3 articles about [3-Bromo-4-(3-diethylamino-propoxy)-phenyl]-(1-bromo-2-ethyl-indolizin-3-yl)-methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.1%

: 77832-72-5
1-bromo-2-ethyl-3-(3-bromo-4-hydroxy-benzoyl)-indolizine

: 104-77-8
3-diethylaminopropyl chloride

: 79286-30-9
[3-Bromo-4-(3-diethylamino-propoxy)-phenyl]-(1-bromo-2-ethyl-indolizin-3-yl)-methanone

Guidance literature:: With potassium carbonate; In acetone; for 20h; Heating;

Reference yield:

: 88265-22-9
2-ethyl-3-(3-bromo-4-tosyloxybenzoyl)-indolizine

: 79286-30-9
[3-Bromo-4-(3-diethylamino-propoxy)-phenyl]-(1-bromo-2-ethyl-indolizin-3-yl)-methanone

Guidance literature:: Multi-step reaction with 3 steps

1: Br₂, sodium acetate trihydrate / dioxane / 1.5 h / 20 - 30 °C

2: 30percent sodium hydroxide / methanol; acetone / 21 h / Heating

3: 74.1 percent / potassium carbonate / acetone / 20 h / Heating

With sodium hydroxide; bromine; sodium acetate; potassium carbonate; In 1,4-dioxane; methanol; acetone;

Reference yield:

: Toluene-4-sulfonic acid 2-bromo-4-(1-bromo-2-ethyl-indolizine-3-carbonyl)-phenyl ester

: 79286-30-9
[3-Bromo-4-(3-diethylamino-propoxy)-phenyl]-(1-bromo-2-ethyl-indolizin-3-yl)-methanone

Guidance literature:: Multi-step reaction with 2 steps

1: 30percent sodium hydroxide / methanol; acetone / 21 h / Heating

2: 74.1 percent / potassium carbonate / acetone / 20 h / Heating

With sodium hydroxide; potassium carbonate; In methanol; acetone;