7,12-bis(trimethylsilyl)-7,12-dihydro-7,12-epoxybenz-anthracene

Base Information

• Chemical Name: 7,12-bis(trimethylsilyl)-7,12-dihydro-7,12-epoxybenz
• Molecular Formula: C₂₄H₂₈OSi₂
• Molecular Weight: 388.657

Synonyms:7,12-bis(trimethylsilyl)-7,12-dihydro-7,12-epoxybenz-anthracene

Chemical Property of 7,12-bis(trimethylsilyl)-7,12-dihydro-7,12-epoxybenz

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

There total 1 articles about 7,12-bis(trimethylsilyl)-7,12-dihydro-7,12-epoxybenz-anthracene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-Ethoxy-1,3-dihydroisobenzofuran (75802-19-6) → 7,12-bis(trimethylsilyl)-7,12-dihydro-7,12-epoxybenz-anthracene (96913-95-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) diisopropylamine, n-BuLi / 1.) ether, hexane, O deg C, 2 h, 2.) ether, hexane, RT

2: 70 percent / LTMP / diethyl ether; hexane / 14 h

With n-butyllithium; 2,2,6,6-tetramethylpiperidinyl-lithium; diisopropylamine; In diethyl ether; hexane;

DOI:10.1021/jo00215a031

upstream raw materials:

1-Ethoxy-1,3-dihydroisobenzofuran

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