(3R,4S)-6-(tert-butyldimethylsilyloxy)-4-(4-methoxybenzyloxy)-3-methylhexan-1-ol

Base Information

Chemical Name:(3R,4S)-6-(tert-butyldimethylsilyloxy)-4-(4-methoxybenzyloxy)-3-methylhexan-1-ol
CAS No.:1598413-42-3
Molecular Formula:C₂₁H₃₈O₄Si
Molecular Weight:382.616
Hs Code.:

Synonyms:(3R,4S)-6-(tert-butyldimethylsilyloxy)-4-(4-methoxybenzyloxy)-3-methylhexan-1-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3R,4S)-6-(tert-butyldimethylsilyloxy)-4-(4-methoxybenzyloxy)-3-methylhexan-1-ol

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Technology Process of (3R,4S)-6-(tert-butyldimethylsilyloxy)-4-(4-methoxybenzyloxy)-3-methylhexan-1-ol

There total 2 articles about (3R,4S)-6-(tert-butyldimethylsilyloxy)-4-(4-methoxybenzyloxy)-3-methylhexan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: C₂₂H₃₈O₃Si

: 1598413-42-3
(3R,4S)-6-(tert-butyldimethylsilyloxy)-4-(4-methoxybenzyloxy)-3-methylhexan-1-ol

Guidance literature:: C₂₂H₃₈O₃Si; With dimethylsulfide borane complex; In tetrahydrofuran; at 0 - 20 ℃; for 12h; Inert atmosphere;

With dihydrogen peroxide; sodium hydroxide; In water; at 0 - 20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ol500875e

Reference yield: 83.0%

: 148933-64-6
tert-Butyl-[(3S,4R)-3-(4-methoxy-benzyloxy)-4-methyl-hex-5-enyloxy]-dimethyl-silane

: 1598413-42-3
(3R,4S)-6-(tert-butyldimethylsilyloxy)-4-(4-methoxybenzyloxy)-3-methylhexan-1-ol

Guidance literature:: tert-Butyl-[(3S,4R)-3-(4-methoxy-benzyloxy)-4-methyl-hex-5-enyloxy]-dimethyl-silane; With dimethylsulfide borane complex; In tetrahydrofuran; at 0 ℃; for 12h; Inert atmosphere;

With dihydrogen peroxide; sodium hydroxide; In tetrahydrofuran; water; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1007/s12039-019-1600-2

Reference yield:

: 1598413-42-3
(3R,4S)-6-(tert-butyldimethylsilyloxy)-4-(4-methoxybenzyloxy)-3-methylhexan-1-ol

: C₂₁H₃₆O₄Si

Guidance literature:: With sodium hydrogencarbonate; Dess-Martin periodane; In dichloromethane; at 0 - 20 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ol500875e