piperidine-1,4,4-tricarboxylic acid 1-tert-butyl 4-benzyl 4-(3,3-dimethyl-2-oxobutyl) ester

Base Information

Chemical Name:piperidine-1,4,4-tricarboxylic acid 1-tert-butyl 4-benzyl 4-(3,3-dimethyl-2-oxobutyl) ester
CAS No.:1093214-73-3
Molecular Formula:C₂₅H₃₅NO₇
Molecular Weight:461.555
Hs Code.:

Synonyms:piperidine-1,4,4-tricarboxylic acid 1-tert-butyl 4-benzyl 4-(3,3-dimethyl-2-oxobutyl) ester

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Chemical Property of piperidine-1,4,4-tricarboxylic acid 1-tert-butyl 4-benzyl 4-(3,3-dimethyl-2-oxobutyl) ester

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Technology Process of piperidine-1,4,4-tricarboxylic acid 1-tert-butyl 4-benzyl 4-(3,3-dimethyl-2-oxobutyl) ester

There total 3 articles about piperidine-1,4,4-tricarboxylic acid 1-tert-butyl 4-benzyl 4-(3,3-dimethyl-2-oxobutyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 951744-79-9
4-benzyloxycarbonyl-1-tert-butoxycarbonyl-4-piperidinecarboxylic acid

: 5469-26-1
1-Bromopinacolon

: 1093214-73-3
piperidine-1,4,4-tricarboxylic acid 1-tert-butyl 4-benzyl 4-(3,3-dimethyl-2-oxobutyl) ester

Guidance literature:: With potassium carbonate; In butanone; at 20 ℃; for 6h;

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1093214-73-3
piperidine-1,4,4-tricarboxylic acid 1-tert-butyl 4-benzyl 4-(3,3-dimethyl-2-oxobutyl) ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine / dichloromethane / 2 h / 20 °C / pH 9 - 9.5

2.1: potassium carbonate / tetrabutylammomium bromide / toluene / 6 h / Heating / reflux

3.1: potassium hydroxide; water / N,N-dimethyl-formamide / 2 h / 0 °C

3.2: 20 °C

4.1: potassium carbonate / butanone / 6 h / 20 °C

With potassium hydroxide; water; potassium carbonate; triethylamine; tetrabutylammomium bromide; In dichloromethane; N,N-dimethyl-formamide; toluene; butanone;

Reference yield:

: 118753-70-1
N-(tert-butyloxycarbonyl)bis(2-chloroethyl)amine

: 1093214-73-3
piperidine-1,4,4-tricarboxylic acid 1-tert-butyl 4-benzyl 4-(3,3-dimethyl-2-oxobutyl) ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / tetrabutylammomium bromide / toluene / 6 h / Heating / reflux

2.1: potassium hydroxide; water / N,N-dimethyl-formamide / 2 h / 0 °C

2.2: 20 °C

3.1: potassium carbonate / butanone / 6 h / 20 °C

With potassium hydroxide; water; potassium carbonate; tetrabutylammomium bromide; In N,N-dimethyl-formamide; toluene; butanone;