C₄₆H₆₅N₃O₈

Base Information

Chemical Name:C₄₆H₆₅N₃O₈
CAS No.:945496-83-3
Molecular Formula:C₄₆H₆₅N₃O₈
Molecular Weight:788.037
Hs Code.:

C<sub>46</sub>H<sub>65</sub>N<sub>3</sub>O<sub>8</sub>

Synonyms:C₄₆H₆₅N₃O₈

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Chemical Property of C₄₆H₆₅N₃O₈

Chemical Property:

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Technology Process of C₄₆H₆₅N₃O₈

There total 14 articles about C₄₆H₆₅N₃O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₁H₂₄N₂O₅

: 945496-83-3
C₄₆H₆₅N₃O₈

Guidance literature:: Multi-step reaction with 7 steps

1.1: TFA / CH₂Cl₂ / 1 h / 20 °C

1.2: 4.50 g / benzaldehyde / ethyl acetate / 0 - 20 °C

2.1: hydroxylamine hydrochloride / methanol / 0.33 h / 60 °C

3.1: SOCl₂ / 16 h / 0 - 20 °C

4.1: 2.89 g / NaHCO₃ / CH₂Cl₂ / 16 h / 20 °C

5.1: DIPEA / methanol

6.1: 100 percent / H₂ / Pd-C / methanol / 0.75 h / 20 °C

7.1: 0.425 g / EDC; HOAt; DMAP / dimethylformamide / 16 h / 20 °C

With dmap; thionyl chloride; 1-hydroxy-7-aza-benzotriazole; hydroxylamine hydrochloride; hydrogen; sodium hydrogencarbonate; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; palladium on activated charcoal; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/b703116e

Reference yield:

: 440679-63-0,945496-80-0
C₂₁H₂₄N₂O₅

: 945496-83-3
C₄₆H₆₅N₃O₈

Guidance literature:: Multi-step reaction with 6 steps

1: hydroxylamine hydrochloride / methanol / 0.33 h / 60 °C

2: SOCl₂ / 16 h / 0 - 20 °C

3: 2.89 g / NaHCO₃ / CH₂Cl₂ / 16 h / 20 °C

4: DIPEA / methanol

5: 100 percent / H₂ / Pd-C / methanol / 0.75 h / 20 °C

6: 0.425 g / EDC; HOAt; DMAP / dimethylformamide / 16 h / 20 °C

With dmap; thionyl chloride; 1-hydroxy-7-aza-benzotriazole; hydroxylamine hydrochloride; hydrogen; sodium hydrogencarbonate; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/b703116e

Reference yield:

: 945496-81-1
C₄₇H₈₂N₂O₇

: 945496-83-3
C₄₆H₆₅N₃O₈

Guidance literature:: Multi-step reaction with 3 steps

1: DIPEA / methanol

2: 100 percent / H₂ / Pd-C / methanol / 0.75 h / 20 °C

3: 0.425 g / EDC; HOAt; DMAP / dimethylformamide / 16 h / 20 °C

With dmap; 1-hydroxy-7-aza-benzotriazole; hydrogen; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide;
DOI:10.1039/b703116e