(-)-N-benzyl-α-(<(1S,2R,4R)-2-hydroxy-7,7-dimethylbicyclo<2.2.1>heptan-1-yl>methylthio)maleimide

Base Information

Chemical Name:(-)-N-benzyl-α-(<(1S,2R,4R)-2-hydroxy-7,7-dimethylbicyclo<2.2.1>heptan-1-yl>methylthio)maleimide
CAS No.:132374-46-0
Molecular Formula:C₂₁H₂₅NO₃S
Molecular Weight:371.5
Hs Code.:

Synonyms:(-)-N-benzyl-α-(<(1S,2R,4R)-2-hydroxy-7,7-dimethylbicyclo<2.2.1>heptan-1-yl>methylthio)maleimide

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Chemical Property of (-)-N-benzyl-α-(<(1S,2R,4R)-2-hydroxy-7,7-dimethylbicyclo<2.2.1>heptan-1-yl>methylthio)maleimide

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Technology Process of (-)-N-benzyl-α-(<(1S,2R,4R)-2-hydroxy-7,7-dimethylbicyclo<2.2.1>heptan-1-yl>methylthio)maleimide

There total 3 articles about (-)-N-benzyl-α-(<(1S,2R,4R)-2-hydroxy-7,7-dimethylbicyclo<2.2.1>heptan-1-yl>methylthio)maleimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 132374-44-8,132374-48-2
N-benzyl-α-(<(1S,2R,4R)-2-hydroxy-7,7-dimethylbicyclo<2.2.1>heptan-1-yl>methylthio)succinimide

: 132374-46-0
(-)-N-benzyl-α-(<(1S,2R,4R)-2-hydroxy-7,7-dimethylbicyclo<2.2.1>heptan-1-yl>methylthio)maleimide

Guidance literature:: With N-chloro-succinimide; In tetrachloromethane; for 6h; Heating;
DOI:10.1021/jo00006a005

Reference yield:

: 1631-26-1
1-benzyl-1H-pyrrole-2,5-dione

: 132374-46-0
(-)-N-benzyl-α-(<(1S,2R,4R)-2-hydroxy-7,7-dimethylbicyclo<2.2.1>heptan-1-yl>methylthio)maleimide

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / Et₃N / CH₂Cl₂ / 25 °C

2: 88 percent / N-chlorosuccinimide / CCl₄ / Heating

With N-chloro-succinimide; triethylamine; In tetrachloromethane; dichloromethane;

Reference yield:

: 71242-58-5
(1S,2R,4R)-(-)-10-mercaptoisoboneol

: 132374-46-0
(-)-N-benzyl-α-(<(1S,2R,4R)-2-hydroxy-7,7-dimethylbicyclo<2.2.1>heptan-1-yl>methylthio)maleimide

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / Et₃N / CH₂Cl₂ / 25 °C

2: 88 percent / N-chlorosuccinimide / CCl₄ / Heating

With N-chloro-succinimide; triethylamine; In tetrachloromethane; dichloromethane;