C₄₂H₅₈O₇Si

Base Information

Chemical Name:C₄₂H₅₈O₇Si
CAS No.:1365268-48-9
Molecular Formula:C₄₂H₅₈O₇Si
Molecular Weight:703.004
Hs Code.:

C<sub>42</sub>H<sub>58</sub>O<sub>7</sub>Si

Synonyms:C₄₂H₅₈O₇Si

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Chemical Property of C₄₂H₅₈O₇Si

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Technology Process of C₄₂H₅₈O₇Si

There total 10 articles about C₄₂H₅₈O₇Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 79-20-9
acetic acid methyl ester

: 1365268-33-2
C₃₉H₅₂O₅Si

: 1365268-48-9
C₄₂H₅₈O₇Si

Guidance literature:: acetic acid methyl ester; With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃;

C₃₉H₅₂O₅Si; In tetrahydrofuran; at -78 ℃;
DOI:10.1016/j.tetlet.2012.01.058

Reference yield:

: C₁₉H₂₄O₂

: 1365268-48-9
C₄₂H₅₈O₇Si

Guidance literature:: Multi-step reaction with 9 steps

1.1: toluene-4-sulfonic acid / benzene / Reflux

2.1: n-butyllithium / tetrahydrofuran / -78 °C

2.2: -78 - 20 °C

3.1: sodium bis(2-methoxyethoxy)aluminium dihydride / diethyl ether / 20 °C

3.2: 0 °C

3.3: -78 °C

4.1: 1H-imidazole / dichloromethane / 20 °C

5.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / 60 °C

6.1: diisobutylaluminium hydride / dichloromethane / -78 °C

7.1: hydrogenchloride; water / tetrahydrofuran / 20 °C

8.1: N-ethyl-N,N-diisopropylamine / 1,2-dichloro-ethane / 50 °C

9.1: lithium diisopropyl amide / tetrahydrofuran / -78 °C

9.2: -78 °C

With 1H-imidazole; hydrogenchloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; water; diisobutylaluminium hydride; toluene-4-sulfonic acid; triethylamine; N-ethyl-N,N-diisopropylamine; sodium bis(2-methoxyethoxy)aluminium dihydride; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; dichloromethane; 1,2-dichloro-ethane; benzene;
DOI:10.1016/j.tetlet.2012.01.058

Reference yield:

: 1365268-47-8
C₃₇H₄₈O₄Si

: 1365268-48-9
C₄₂H₅₈O₇Si

Guidance literature:: Multi-step reaction with 2 steps

1.1: N-ethyl-N,N-diisopropylamine / 1,2-dichloro-ethane / 50 °C

2.1: lithium diisopropyl amide / tetrahydrofuran / -78 °C

2.2: -78 °C

With N-ethyl-N,N-diisopropylamine; lithium diisopropyl amide; In tetrahydrofuran; 1,2-dichloro-ethane;
DOI:10.1016/j.tetlet.2012.01.058