(1S,2S,3S,4S)-2-(4-bromophenyl)-4-hydroxy-3-nitro-cyclohexanecarbaldehyde

Base Information

Chemical Name:(1S,2S,3S,4S)-2-(4-bromophenyl)-4-hydroxy-3-nitro-cyclohexanecarbaldehyde
CAS No.:947740-45-6
Molecular Formula:C₁₃H₁₄BrNO₄
Molecular Weight:328.162
Hs Code.:

Synonyms:(1S,2S,3S,4S)-2-(4-bromophenyl)-4-hydroxy-3-nitro-cyclohexanecarbaldehyde

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S,2S,3S,4S)-2-(4-bromophenyl)-4-hydroxy-3-nitro-cyclohexanecarbaldehyde

Chemical Property:

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Technology Process of (1S,2S,3S,4S)-2-(4-bromophenyl)-4-hydroxy-3-nitro-cyclohexanecarbaldehyde

There total 3 articles about (1S,2S,3S,4S)-2-(4-bromophenyl)-4-hydroxy-3-nitro-cyclohexanecarbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 85571-98-8
2,5-dihydroxy-3,4-dihydrofuran

: 947740-45-6
(1S,2S,3S,4S)-2-(4-bromophenyl)-4-hydroxy-3-nitro-cyclohexanecarbaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 64 percent / (S)-2-diphenyltrimethylsiloxymethylpyrrolidine / H₂O; tetrahydrofuran / 4 h / 20 °C

2: 1,8-diazabicyclo[5.4.0]-undec-7-ene / methanol / 20 °C

With 1,8-diazabicyclo[5.4.0]undec-7-ene; (S)-2-diphenyltrimethylsiloxymethylpyrrolidine; In tetrahydrofuran; methanol; water;
DOI:10.1002/anie.200700909

Reference yield:

: 3156-37-4,5153-71-9
(E)-1-bromo-4-(2-nitrovinyl)benzene

: 947740-45-6
(1S,2S,3S,4S)-2-(4-bromophenyl)-4-hydroxy-3-nitro-cyclohexanecarbaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 64 percent / (S)-2-diphenyltrimethylsiloxymethylpyrrolidine / H₂O; tetrahydrofuran / 4 h / 20 °C

2: 1,8-diazabicyclo[5.4.0]-undec-7-ene / methanol / 20 °C

With 1,8-diazabicyclo[5.4.0]undec-7-ene; (S)-2-diphenyltrimethylsiloxymethylpyrrolidine; In tetrahydrofuran; methanol; water;
DOI:10.1002/anie.200700909

Reference yield:

: 947740-36-5
(1R,2S,3S,4R)-4-hydroxy-3-nitro-2-(4-bromophenyl)cyclohexanecarbaldehyde

: 947740-45-6
(1S,2S,3S,4S)-2-(4-bromophenyl)-4-hydroxy-3-nitro-cyclohexanecarbaldehyde

: 2-(4-bromophenyl)-4-hydroxy-3-nitro-cyclohexanecarbaldehyde

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In methanol; at 20 ℃; Title compound not separated from byproducts.;
DOI:10.1002/anie.200700909