3,5-Dichloro-4-methoxybenzoyl chloride

Base Information

• Chemical Name: 3,5-Dichloro-4-methoxybenzoyl chloride
• CAS No.: 29568-76-1
• Molecular Formula: C8H5 Cl3 O2
• Molecular Weight: 239.485
• Hs Code.: 2918990090
• DSSTox Substance ID: DTXSID80397026
• Wikidata: Q82198039
• Mol file: 29568-76-1.mol

Synonyms:3,5-dichloro-4-methoxybenzoyl chloride;29568-76-1;Benzoyl chloride, 3,5-dichloro-4-methoxy-;3,5-DICHLORO-4-METHOXY-BENZOYL CHLORIDE;SCHEMBL985523;DTXSID80397026;XWIGDNQZKUVSQD-UHFFFAOYSA-N;AC5825;MFCD02063082;AKOS000289066;AS-65246;BB 0244158;FT-0742626;J-017567

Chemical Property of 3,5-Dichloro-4-methoxybenzoyl chloride

Chemical Property:

• Vapor Pressure: 0.000495mmHg at 25°C
• Melting Point: 63-65℃
• Refractive Index: 1.56
• Boiling Point: 313.5°C at 760 mmHg
• Flash Point: 136°C
• PSA: 26.30000
• Density: 1.462g/cm³
• LogP: 3.38100
• XLogP3: 3.9
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 2
• Exact Mass: 237.935512
• Heavy Atom Count: 13
• Complexity: 186

Purity/Quality:

99% ^*data from raw suppliers

3,5-DICHLORO-4-METHOXYBENZOYL CHLORIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC1=C(C=C(C=C1Cl)C(=O)Cl)Cl

Technology Process of 3,5-Dichloro-4-methoxybenzoyl chloride

There total 1 articles about 3,5-Dichloro-4-methoxybenzoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,5-dichloro-4-methoxybenzoic acid (37908-97-7) → 3,5-Dichloro-4-methoxybenzoyl chloride (29568-76-1)

Guidance literature:

With thionyl chloride; for 3h; Heating;

DOI:10.1007/BF00759051

Reference yield: 86.0%

20'-aminovinblastine + 3,5-Dichloro-4-methoxybenzoyl chloride (29568-76-1) → C54H63Cl2N5O10

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 23 ℃; for 2h; Inert atmosphere;

DOI:10.1021/acs.jmedchem.7b00958

Reference yield: 56.6%

3,5-Dichloro-4-methoxybenzoyl chloride (29568-76-1) + ethyl acetoacetate (141-97-9) → 3,5-Dichloro-4-methoxybenzoylacetic acid ethyl ester (114194-96-6)

Guidance literature:

With sodium hydroxide; In toluene; 1.) room temp., 1.5 h, 2.) 27-33 deg C, 1 h;

DOI:10.1007/BF00759051

upstream raw materials:

3,5-dichloro-4-methoxybenzoic acid

Downstream raw materials:

3,5-Dichloro-4-methoxybenzoylacetic acid ethyl ester

(Dichloro-3,5-methoxy-4-phenyl)-1-diazo-2-ethanon

2-(3,5-Dichloro-4-methoxy-phenyl)-5-hydroxy-benzofuran-3-carboxylic acid ethyl ester

(3,5-dichloro-4-methoxy-phenyl)-acetic acid amide

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