ethyl 2-<<3-phenyl-(E)-2-propenyl>oxy>-2-chloro-3,3,3-trifluoropropanoate

Base Information

Chemical Name:ethyl 2-<<3-phenyl-(E)-2-propenyl>oxy>-2-chloro-3,3,3-trifluoropropanoate
CAS No.:168101-87-9
Molecular Formula:C₁₄H₁₄ClF₃O₃
Molecular Weight:322.712
Hs Code.:

Synonyms:ethyl 2-<<3-phenyl-(E)-2-propenyl>oxy>-2-chloro-3,3,3-trifluoropropanoate

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Chemical Property of ethyl 2-<<3-phenyl-(E)-2-propenyl>oxy>-2-chloro-3,3,3-trifluoropropanoate

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Technology Process of ethyl 2-<<3-phenyl-(E)-2-propenyl>oxy>-2-chloro-3,3,3-trifluoropropanoate

There total 3 articles about ethyl 2-<<3-phenyl-(E)-2-propenyl>oxy>-2-chloro-3,3,3-trifluoropropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4407-36-7
(2E)-3-phenyl-2-propen-1-ol

: 168101-87-9
ethyl 2-<<3-phenyl-(E)-2-propenyl>oxy>-2-chloro-3,3,3-trifluoropropanoate

Guidance literature:: Multi-step reaction with 2 steps

1: benzene / 0.5 h / Ambient temperature

2: SOCl₂ / benzene; pyridine / 0.5 h / 0 °C

With thionyl chloride; In pyridine; benzene;
DOI:10.1021/jo00125a013

Reference yield:

: 1026684-27-4
3,3,3-Trifluoro-2-hydroxy-2-((E)-3-phenyl-allyloxy)-propionic acid ethyl ester

: 168101-87-9
ethyl 2-<<3-phenyl-(E)-2-propenyl>oxy>-2-chloro-3,3,3-trifluoropropanoate

Guidance literature:: With thionyl chloride; In pyridine; benzene; at 0 ℃; for 0.5h; Yield given;
DOI:10.1021/jo00125a013

Reference yield:

: 13081-18-0
ethyl-3,3,3-trifluoropyruvate

: 168101-87-9
ethyl 2-<<3-phenyl-(E)-2-propenyl>oxy>-2-chloro-3,3,3-trifluoropropanoate

Guidance literature:: Multi-step reaction with 2 steps

1: benzene / 0.5 h / Ambient temperature

2: SOCl₂ / benzene; pyridine / 0.5 h / 0 °C

With thionyl chloride; In pyridine; benzene;
DOI:10.1021/jo00125a013