1-phenyl-9H-fluorene

Base Information

• Chemical Name: 1-phenyl-9H-fluorene
• CAS No.: 66972-63-2
• Molecular Formula: C₁₉H₁₄
• Molecular Weight: 242.32
• Mol file: 66972-63-2.mol

Synonyms:1-phenyl-9H-fluorene

Chemical Property of 1-phenyl-9H-fluorene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-phenyl-9H-fluorene

There total 11 articles about 1-phenyl-9H-fluorene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

2-bromo-9H-fluorene (1133-80-8) + phenylboronic acid (98-80-6) → 1-phenyl-9H-fluorene (66972-63-2)

Guidance literature:

2-bromo-9H-fluorene; phenylboronic acid; With p-xylene-2-sulphonic acid sodium salt; In water; at 28 ℃; for 0.0833333h;

With palladium 10% on activated carbon; potassium carbonate; In water; at 28 ℃; for 7h;

DOI:10.1039/c5gc02314a

Reference yield: 69.0%

1-phenyl-9H-fluoren-9-one (5501-35-9) → 1-phenyl-9H-fluorene (66972-63-2)

Guidance literature:

1-phenyl-9H-fluoren-9-one; With hydrazine hydrate; In diethylene glycol; at 100 ℃; Inert atmosphere;

With potassium hydroxide; In water; at 130 ℃; for 6h; Inert atmosphere;

DOI:10.1002/chem.201700570

Reference yield:

1-phenyl-1,2,3,9a-tetrahydro-fluoren-3-ol (102018-22-4) → 1-phenyl-9H-fluorene (66972-63-2)

Guidance literature:

With sulfur; at 220 ℃;

upstream raw materials:

1-phenyl-1,2,3,9a-tetrahydro-fluoren-3-ol

7,7-dichloro-bicyclo[4.1.0]heptane

benzene

1-phenyl-9H-fluoren-9-one

Downstream raw materials:

1-phenyl-9H-fluoren-9-one