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C18H34O3Si

Base Information
  • Chemical Name:C18H34O3Si
  • CAS No.:1356926-06-1
  • Molecular Formula:C18H34O3Si
  • Molecular Weight:326.552
  • Hs Code.:
C<sub>18</sub>H<sub>34</sub>O<sub>3</sub>Si

Synonyms:C18H34O3Si

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Chemical Property of C18H34O3Si
Chemical Property:
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Technology Process of C18H34O3Si

There total 8 articles about C18H34O3Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With diisobutylaluminium hydride; In dichloromethane; at 0 ℃; for 1h;
DOI:10.1016/j.tetlet.2011.12.015
Guidance literature:
Multi-step reaction with 4 steps
1: oxygen; palladium diacetate / dimethyl sulfoxide / 72 h / 55 °C
2: sodium tetrahydroborate; cerium(III) chloride heptahydrate / methanol / 0.25 h
3: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N,N,N,N,N-hexamethylphosphoric triamide / 3 h / -15 °C
4: diisobutylaluminium hydride / dichloromethane / 1 h / 0 °C
With sodium tetrahydroborate; cerium(III) chloride heptahydrate; oxygen; palladium diacetate; tetra-(n-butyl)ammonium iodide; sodium hydride; diisobutylaluminium hydride; In methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane; dimethyl sulfoxide; 2: Luche reduction;
DOI:10.1016/j.tetlet.2011.12.015
Guidance literature:
Multi-step reaction with 2 steps
1: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N,N,N,N,N-hexamethylphosphoric triamide / 3 h / -15 °C
2: diisobutylaluminium hydride / dichloromethane / 1 h / 0 °C
With tetra-(n-butyl)ammonium iodide; sodium hydride; diisobutylaluminium hydride; In N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane;
DOI:10.1016/j.tetlet.2011.12.015
upstream raw materials:

C17H30O4Si

C17H32O4Si

C20H36O4Si

C17H32O4Si

Downstream raw materials:

C18H32O3Si

C19H32O2Si

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