Bicyclo[2.2.1]heptane-2,3-dithiol

Base Information

Chemical Name:Bicyclo[2.2.1]heptane-2,3-dithiol
CAS No.:133209-22-0
Molecular Formula:C7H12S2
Molecular Weight:160.30018
Hs Code.:
DSSTox Substance ID:DTXSID60342397
Nikkaji Number:J1.436.270C
Mol file:133209-22-0.mol

Synonyms:Bicyclo[2.2.1]heptane-2,3-dithiol;133209-22-0;Bicyclo[2.2.1]heptane-2,3-dithiol (9CI);Norbornane-2,3-dithiol;SCHEMBL16406138;DTXSID60342397

Suppliers and Price of Bicyclo[2.2.1]heptane-2,3-dithiol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of Bicyclo[2.2.1]heptane-2,3-dithiol

Chemical Property:

PSA：77.60000
LogP:2.01310
XLogP3:2.1
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:160.03804273
Heavy Atom Count:9
Complexity:110

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CC2CC1C(C2S)S

Technology Process of Bicyclo[2.2.1]heptane-2,3-dithiol

There total 2 articles about Bicyclo[2.2.1]heptane-2,3-dithiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 56904-67-7,96614-16-3
bicyclo<2.2.1>heptane-cis-2,3-dithiol thionocarbonates

: 23657-28-5,96556-88-6,133209-22-0
cis-bicyclo<2.2.1>heptane-2,3-dithiol

Guidance literature:: With sodium hydroxide; In methanol; water; for 20h; Heating;
DOI:10.1021/ja00300a016

Reference yield:

: 5024-92-0
2-morpholinobicyclo<2.2.1>hept-2-en

: 23657-28-5,96556-88-6,133209-22-0
cis-bicyclo<2.2.1>heptane-2,3-dithiol

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N

2: NaOH / methanol; H₂O / 20 h / Heating

With sodium hydroxide; triethylamine; In methanol; water;
DOI:10.1021/ja00300a016

Reference yield:

: 133209-22-0
Bicyclo[2.2.1]heptane-2,3-dithiol

: C₄₈H₇₀O₂PtS₈Si₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: toluene-4-sulfonic acid / hexane / 85 h / 80 °C / Inert atmosphere

2.1: sodium hydroxide / butan-1-ol / 4 h / 70 °C / Inert atmosphere

2.2: 2.5 h / 110 °C / Inert atmosphere

With toluene-4-sulfonic acid; sodium hydroxide; In hexane; butan-1-ol;