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Carbamic acid, [(1S)-1-(aminocarbonyl)propyl]-, 1,1-dimethylethyl ester (9CI)

Base Information Edit
  • Chemical Name:Carbamic acid, [(1S)-1-(aminocarbonyl)propyl]-, 1,1-dimethylethyl ester (9CI)
  • CAS No.:148528-89-6
  • Molecular Formula:C9H18 N2 O3
  • Molecular Weight:202.254
  • Hs Code.:
  • Mol file:148528-89-6.mol
Carbamic acid, [(1S)-1-(aminocarbonyl)propyl]-, 1,1-dimethylethyl ester (9CI)

Synonyms:Carbamicacid, [1-(aminocarbonyl)propyl]-, 1,1-dimethylethyl ester, (S)-; tert-Butyl((1S)-1-carbamoylpropyl)carbamate

Suppliers and Price of Carbamic acid, [(1S)-1-(aminocarbonyl)propyl]-, 1,1-dimethylethyl ester (9CI)
Supply Marketing:Edit
Business phase:
The product has achieved commercial mass production*data from LookChem market partment
Manufacturers and distributors:
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Chemical Property of Carbamic acid, [(1S)-1-(aminocarbonyl)propyl]-, 1,1-dimethylethyl ester (9CI) Edit
Chemical Property:
  • PSA:81.42000 
  • LogP:1.86620 
Purity/Quality:
Safty Information:
  • Pictogram(s):  
  • Hazard Codes: 
MSDS Files:

SDS file from LookChem

Useful:
Technology Process of Carbamic acid, [(1S)-1-(aminocarbonyl)propyl]-, 1,1-dimethylethyl ester (9CI)

There total 5 articles about Carbamic acid, [(1S)-1-(aminocarbonyl)propyl]-, 1,1-dimethylethyl ester (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
Boc-Abu; With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl-formamide; for 0.166667h;
With 1,1,1,3,3,3-hexamethyl-disilazane; In dichloromethane; N,N-dimethyl-formamide; at 20 ℃; for 1h;
With hydrogenchloride; water; In ethyl acetate;
Guidance literature:
With ammonium hydroxide; In tetrahydrofuran; at -15 ℃; for 2h; Yield given;
DOI:10.1016/0223-5234(92)90027-X
Guidance literature:
With ammonium hydroxide; In tetrahydrofuran;
DOI:10.1016/S0960-894X(03)00495-5
upstream raw materials:

di-tert-butyl dicarbonate

Boc-Abu

Downstream raw materials:

(S)-2-amino-butanamide hydrochloride

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