2,4-Diazido-5-((2S,3R,4S,5S,6S)-3,5-diazido-4-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxy)-cyclohexanol

Base Information

• Chemical Name: 2,4-Diazido-5-((2S,3R,4S,5S,6S)-3,5-diazido-4-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxy)-cyclohexanol
• CAS No.: 636560-75-3
• Molecular Formula: C₂₆H₃₀N₁₂O₅
• Molecular Weight: 590.602

Synonyms:2,4-Diazido-5-((2S,3R,4S,5S,6S)-3,5-diazido-4-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxy)-cyclohexanol

Chemical Property of 2,4-Diazido-5-((2S,3R,4S,5S,6S)-3,5-diazido-4-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxy)-cyclohexanol

Chemical Property:

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Technology Process of 2,4-Diazido-5-((2S,3R,4S,5S,6S)-3,5-diazido-4-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxy)-cyclohexanol

There total 1 articles about 2,4-Diazido-5-((2S,3R,4S,5S,6S)-3,5-diazido-4-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxy)-cyclohexanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

meso-(1R,3S,4S,6R)-4,6-diazidocyclohexane-1,3-diol (69048-60-8) + (2S,3S,4S,5R,6S)-3,5-Diazido-4-benzyloxy-2-benzyloxymethyl-6-ethylsulfanyl-tetrahydro-pyran (635310-01-9) → 2,4-Diazido-5-((2S,3R,4S,5S,6S)-3,5-diazido-4-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxy)-cyclohexanol (636560-75-3) + C46H50N18O8

Guidance literature:

With N-iodo-succinimide; 4 A molecular sieve; silver trifluoromethanesulfonate; In diethyl ether; dichloromethane; toluene; at -40 ℃; for 5h;

DOI:10.1055/s-2003-40351

Reference yield: 80.0%

(2S,3R,4S,5R,6S)-3,5-Diazido-4-benzyloxy-2-benzyloxymethyl-6-ethylsulfanyl-tetrahydro-pyran (635309-99-8) + 2,4-Diazido-5-((2S,3R,4S,5S,6S)-3,5-diazido-4-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxy)-cyclohexanol (636560-75-3) → C46H50N18O8

Guidance literature:

With N-iodo-succinimide; 4 A molecular sieve; silver trifluoromethanesulfonate; In diethyl ether; dichloromethane; toluene; at -40 ℃; for 5h;

DOI:10.1055/s-2003-40351

Reference yield: 49.0%

2,4-Diazido-5-((2S,3R,4S,5S,6S)-3,5-diazido-4-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxy)-cyclohexanol (636560-75-3) → (2S,3R,4S,5S,6S)-3,5-Diamino-2-(2,4-diamino-5-hydroxy-cyclohexyloxy)-6-hydroxymethyl-tetrahydro-pyran-4-ol

Guidance literature:

With hydrogen; acetic acid; palladium dihydroxide; In methanol; at 20 ℃; for 7h;

DOI:10.1055/s-2003-40351

upstream raw materials:

meso-(1R,3S,4S,6R)-4,6-diazidocyclohexane-1,3-diol

(2S,3S,4S,5R,6S)-3,5-Diazido-4-benzyloxy-2-benzyloxymethyl-6-ethylsulfanyl-tetrahydro-pyran

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