C₃₅H₃₁N₃O₅S

Base Information

Chemical Name:C₃₅H₃₁N₃O₅S
CAS No.:1338711-15-1
Molecular Formula:C₃₅H₃₁N₃O₅S
Molecular Weight:605.714
Hs Code.:

C<sub>35</sub>H<sub>31</sub>N<sub>3</sub>O<sub>5</sub>S

Synonyms:C₃₅H₃₁N₃O₅S

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Chemical Property of C₃₅H₃₁N₃O₅S

Chemical Property:

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Technology Process of C₃₅H₃₁N₃O₅S

There total 11 articles about C₃₅H₃₁N₃O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1338711-10-6
C₃₆H₃₃N₃O₄S

: 1338711-15-1
C₃₅H₃₁N₃O₅S

Guidance literature:: C₃₆H₃₃N₃O₄S; With osmium(VIII) oxide; 4-methylmorpholine N-oxide; In tetrahydrofuran; water; tert-butyl alcohol; at 20 ℃;

With sodium periodate; In tetrahydrofuran; water; tert-butyl alcohol; at 20 ℃; for 2h;
DOI:10.1021/ol202475r

Reference yield:

: 1338711-08-2
C₂₆H₂₁BrN₂O₃

: 1338711-15-1
C₃₅H₃₁N₃O₅S

Guidance literature:: Multi-step reaction with 7 steps

1.1: hydrazine hydrate / ethanol / Reflux

2.1: methanol / 24 h / 20 °C

3.1: boron trifluoride diethyl etherate / tetrahydrofuran; dichloromethane / 0.25 h / -40 °C / Inert atmosphere

3.2: 4 h / -40 - 20 °C

4.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C / Inert atmosphere

4.2: 0 °C

5.1: tert.-butyl lithium / diethyl ether; pentane / 1.5 h / -40 - 20 °C / Inert atmosphere

6.1: sodium disulfate / tetrahydrofuran / 5 h / 23 °C

6.2: 3 h

7.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / tetrahydrofuran; water; tert-butyl alcohol / 20 °C

7.2: 2 h / 20 °C

With osmium(VIII) oxide; sodium disulfate; boron trifluoride diethyl etherate; tert.-butyl lithium; sodium hydride; hydrazine hydrate; 4-methylmorpholine N-oxide; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; water; mineral oil; tert-butyl alcohol; pentane;
DOI:10.1021/ol202475r

Reference yield:

: 61-54-1
tryptamine

: 1338711-15-1
C₃₅H₃₁N₃O₅S

Guidance literature:: Multi-step reaction with 10 steps

1.1: toluene / Reflux

2.1: pyridinium perbromide hydrobromide / tetrahydrofuran; chloroform / 2.33 h / -10 °C

3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 - 20 °C

3.2: 4 h / 0 - 20 °C

4.1: hydrazine hydrate / ethanol / Reflux

5.1: methanol / 24 h / 20 °C

6.1: boron trifluoride diethyl etherate / tetrahydrofuran; dichloromethane / 0.25 h / -40 °C / Inert atmosphere

6.2: 4 h / -40 - 20 °C

7.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C / Inert atmosphere

7.2: 0 °C

8.1: tert.-butyl lithium / diethyl ether; pentane / 1.5 h / -40 - 20 °C / Inert atmosphere

9.1: sodium disulfate / tetrahydrofuran / 5 h / 23 °C

9.2: 3 h

10.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / tetrahydrofuran; water; tert-butyl alcohol / 20 °C

10.2: 2 h / 20 °C

With osmium(VIII) oxide; sodium disulfate; pyridinium perbromide hydrobromide; boron trifluoride diethyl etherate; tert.-butyl lithium; sodium hydride; hydrazine hydrate; 4-methylmorpholine N-oxide; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; chloroform; water; N,N-dimethyl-formamide; toluene; mineral oil; tert-butyl alcohol; pentane;
DOI:10.1021/ol202475r