(3R)-3-deoxo-11-deoxy-3-methoxy-11-oxo-4-epi-mutilin 14-(N-methyl-N-phenylcarbamate)

Base Information

Chemical Name:(3R)-3-deoxo-11-deoxy-3-methoxy-11-oxo-4-epi-mutilin 14-(N-methyl-N-phenylcarbamate)
CAS No.:193536-90-2
Molecular Formula:C₂₉H₄₁NO₄
Molecular Weight:467.649
Hs Code.:

Synonyms:(3R)-3-deoxo-11-deoxy-3-methoxy-11-oxo-4-epi-mutilin 14-(N-methyl-N-phenylcarbamate)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3R)-3-deoxo-11-deoxy-3-methoxy-11-oxo-4-epi-mutilin 14-(N-methyl-N-phenylcarbamate)

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Technology Process of (3R)-3-deoxo-11-deoxy-3-methoxy-11-oxo-4-epi-mutilin 14-(N-methyl-N-phenylcarbamate)

There total 2 articles about (3R)-3-deoxo-11-deoxy-3-methoxy-11-oxo-4-epi-mutilin 14-(N-methyl-N-phenylcarbamate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 100-61-8
N-methylaniline

: 193536-85-5
(3R,3aS,4R,SR,7S,9R,9aR,12R)-3-methoxy-4,7,9,12-tetramethyl-8-oxo-7-vinyldecahydro-4,9a-propanocyclopenta[8]annulen-5-yl carbonochloridate

: 193536-90-2
(3R)-3-deoxo-11-deoxy-3-methoxy-11-oxo-4-epi-mutilin 14-(N-methyl-N-phenylcarbamate)

Guidance literature:: In dichloromethane;
DOI:10.1016/S0968-0896(00)00338-2

Reference yield:

: 76375-91-2
(3R,3aS,4R,5R,7S,9R,9aR,12R)-5-hydroxy-3-methoxy-4,7,9,12-tetramethyl-7-vinyloctahydro-4,9a-propanocyclopenta[8]annulen-8(9H)-one

: 193536-90-2
(3R)-3-deoxo-11-deoxy-3-methoxy-11-oxo-4-epi-mutilin 14-(N-methyl-N-phenylcarbamate)

Guidance literature:: Multi-step reaction with 2 steps

1: 1.42 g / triethylamine / tetrahydrofuran / 4 h / 20 °C

2: 81 percent / CH₂Cl₂

With triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0968-0896(00)00338-2