Technology Process of MCPA-isooctyl
There total 4 articles about MCPA-isooctyl which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
di(n-butyl)tin oxide;
at 80 - 155 ℃;
for 15h;
under 187.519 Torr;
Concentration;
- Guidance literature:
-
With
macroporous styrenic strong acid cation exchange resin D001H;
at 110 ℃;
for 4h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium hydroxide / toluene / Reflux
1.2: 0.5 h / 50 °C
2.1: Santonox R; silica gel; aluminum (III) chloride; sulfuryl dichloride / 0.5 h / -20 °C
3.1: macroporous styrenic strong acid cation exchange resin D001H / 4 h / 110 °C
With
aluminum (III) chloride; Santonox R; sulfuryl dichloride; silica gel; sodium hydroxide;
In
toluene;