C₃₉H₅₆O₆Si₂

Base Information

Chemical Name:C₃₉H₅₆O₆Si₂
CAS No.:1261152-22-0
Molecular Formula:C₃₉H₅₆O₆Si₂
Molecular Weight:677.041
Hs Code.:

C<sub>39</sub>H<sub>56</sub>O<sub>6</sub>Si<sub>2</sub>

Synonyms:C₃₉H₅₆O₆Si₂

Suppliers and Price of C₃₉H₅₆O₆Si₂

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₃₉H₅₆O₆Si₂

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₃₉H₅₆O₆Si₂

There total 9 articles about C₃₉H₅₆O₆Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₉H₅₆O₅Si₂

: 1261152-22-0
C₃₉H₅₆O₆Si₂

Guidance literature:: With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; In water; tert-butyl alcohol; at 25 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/ja109533y

Reference yield:

: 1261152-44-6
C₃₂H₄₂O₅Si

: 1261152-22-0
C₃₉H₅₆O₆Si₂

Guidance literature:: Multi-step reaction with 9 steps

1.1: 2,6-dimethylpyridine / dichloromethane / 2 h / 25 °C / Inert atmosphere

2.1: 10-camphorsufonic acid / methanol / 3 h / 25 °C / Inert atmosphere

3.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 0 - 25 °C / Inert atmosphere; Molecular sieve

4.1: sodium hexamethyldisilazane / tetrahydrofuran; toluene / 0.5 h / 0 °C / Inert atmosphere

4.2: -78 - 0 °C / Inert atmosphere

5.1: p-toluenesulfonic acid monohydrate / methanol; dichloromethane / 3 h / 25 °C / Inert atmosphere

6.1: 1H-imidazole / dichloromethane / 1 h / 25 °C / Inert atmosphere

7.1: bis(cyclohexanyl)borane / tetrahydrofuran / 0 - 25 °C / Inert atmosphere

7.2: 1 h / 0 °C / Inert atmosphere

8.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 3 h / 25 °C / Inert atmosphere

9.1: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / water; tert-butyl alcohol / 0.5 h / 25 °C / Inert atmosphere

With 1H-imidazole; 2,6-dimethylpyridine; sodium chlorite; sodium dihydrogenphosphate; tetrapropylammonium perruthennate; 2-methyl-but-2-ene; bis(cyclohexanyl)borane; 10-camphorsufonic acid; p-toluenesulfonic acid monohydrate; sodium hexamethyldisilazane; sodium hydrogencarbonate; Dess-Martin periodane; 4-methylmorpholine N-oxide; In tetrahydrofuran; methanol; dichloromethane; water; toluene; tert-butyl alcohol; 4.1: Wittig reaction / 4.2: Wittig reaction / 7.1: Hydroboration reaction;
DOI:10.1021/ja109533y

Reference yield:

: C₃₈H₅₄O₅Si₂

: 1261152-22-0
C₃₉H₅₆O₆Si₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hexamethyldisilazane / tetrahydrofuran; toluene / 0.5 h / 0 °C / Inert atmosphere

1.2: -78 - 0 °C / Inert atmosphere

2.1: p-toluenesulfonic acid monohydrate / methanol; dichloromethane / 3 h / 25 °C / Inert atmosphere

3.1: 1H-imidazole / dichloromethane / 1 h / 25 °C / Inert atmosphere

4.1: bis(cyclohexanyl)borane / tetrahydrofuran / 0 - 25 °C / Inert atmosphere

4.2: 1 h / 0 °C / Inert atmosphere

5.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 3 h / 25 °C / Inert atmosphere

6.1: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / water; tert-butyl alcohol / 0.5 h / 25 °C / Inert atmosphere

With 1H-imidazole; sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; bis(cyclohexanyl)borane; p-toluenesulfonic acid monohydrate; sodium hexamethyldisilazane; sodium hydrogencarbonate; Dess-Martin periodane; In tetrahydrofuran; methanol; dichloromethane; water; toluene; tert-butyl alcohol; 1.1: Wittig reaction / 1.2: Wittig reaction / 4.1: Hydroboration reaction;
DOI:10.1021/ja109533y