C₄₀H₅₂N₂O₇

Base Information

Chemical Name:C₄₀H₅₂N₂O₇
CAS No.:1343505-27-0
Molecular Formula:C₄₀H₅₂N₂O₇
Molecular Weight:672.862
Hs Code.:

C<sub>40</sub>H<sub>52</sub>N<sub>2</sub>O<sub>7</sub>

Synonyms:C₄₀H₅₂N₂O₇

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Chemical Property of C₄₀H₅₂N₂O₇

Chemical Property:

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Technology Process of C₄₀H₅₂N₂O₇

There total 8 articles about C₄₀H₅₂N₂O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1343505-22-5
C₄₆H₆₆N₂O₇Si

: 1343505-27-0
C₄₀H₅₂N₂O₇

Guidance literature:: With CSA; In methanol; dichloromethane; at 0 ℃; for 1h;
DOI:10.1016/j.tetlet.2011.08.158

Reference yield:

: 1343505-16-7
C₁₈H₂₈O₄

: 1343505-27-0
C₄₀H₅₂N₂O₇

Guidance literature:: Multi-step reaction with 6 steps

1: 2,6-dimethylpyridine / dichloromethane / 0.75 h / 20 °C

2: diisobutylaluminium hydride / dichloromethane / 2 h / -40 - -10 °C

3: Dess-Martin periodane / dichloromethane / 1 h / 0 - 20 °C

4: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 1 h

5: 1-ethyl-piperidine; HATU / acetonitrile / 12 h / 0 - 20 °C

6: CSA / methanol; dichloromethane / 1 h / 0 °C

With 1-ethyl-piperidine; 2,6-dimethylpyridine; sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; diisobutylaluminium hydride; Dess-Martin periodane; HATU; In methanol; dichloromethane; water; acetonitrile; tert-butyl alcohol;
DOI:10.1016/j.tetlet.2011.08.158

Reference yield:

: 1343505-09-8
C₁₈H₃₀O₄

: 1343505-27-0
C₄₀H₅₂N₂O₇

Guidance literature:: Multi-step reaction with 7 steps

1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 2 h / -10 °C / Molecular sieve

2: 2,6-dimethylpyridine / dichloromethane / 0.75 h / 20 °C

3: diisobutylaluminium hydride / dichloromethane / 2 h / -40 - -10 °C

4: Dess-Martin periodane / dichloromethane / 1 h / 0 - 20 °C

5: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 1 h

6: 1-ethyl-piperidine; HATU / acetonitrile / 12 h / 0 - 20 °C

7: CSA / methanol; dichloromethane / 1 h / 0 °C

With 1-ethyl-piperidine; 2,6-dimethylpyridine; sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; diisobutylaluminium hydride; Dess-Martin periodane; HATU; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In methanol; dichloromethane; water; acetonitrile; tert-butyl alcohol;
DOI:10.1016/j.tetlet.2011.08.158