4,6-dibutoxyisophthalic acid

Base Information

Chemical Name:4,6-dibutoxyisophthalic acid
CAS No.:1454709-95-5
Molecular Formula:C₁₆H₂₂O₆
Molecular Weight:310.347
Hs Code.:

Synonyms:4,6-dibutoxyisophthalic acid

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Chemical Property of 4,6-dibutoxyisophthalic acid

Chemical Property:

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Technology Process of 4,6-dibutoxyisophthalic acid

There total 1 articles about 4,6-dibutoxyisophthalic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1454709-89-7
dimethyl 4,6-dibutoxyisophthalate

: 1454709-95-5
4,6-dibutoxyisophthalic acid

Guidance literature:: With water; potassium hydroxide; In methanol; at 80 ℃; for 24h;
DOI:10.1021/ol4021207

Reference yield:

: 1454709-95-5
4,6-dibutoxyisophthalic acid

: 1454710-11-2
C₄₆H₆₈N₆O₆

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 2 h

2: triethylamine / dichloromethane / 0 °C / Inert atmosphere

3: trifluoroacetic acid / 20 °C

With oxalyl dichloride; triethylamine; N,N-dimethyl-formamide; trifluoroacetic acid; In dichloromethane;
DOI:10.1021/ol4021207

Reference yield:

: 1454709-95-5
4,6-dibutoxyisophthalic acid

: 1454710-07-6
C₅₆H₈₄N₆O₁₀

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 2 h

2: triethylamine / dichloromethane / 0 °C / Inert atmosphere

With oxalyl dichloride; triethylamine; N,N-dimethyl-formamide; In dichloromethane;
DOI:10.1021/ol4021207