trans-2(e),6(a)-diphenyl-4,4-(ethylenedioxy)cyclohexane-1(e)-carbonitrile

Base Information

Chemical Name:trans-2(e),6(a)-diphenyl-4,4-(ethylenedioxy)cyclohexane-1(e)-carbonitrile
CAS No.:111904-75-7
Molecular Formula:C₂₁H₂₁NO₂
Molecular Weight:319.403
Hs Code.:

Synonyms:trans-2(e),6(a)-diphenyl-4,4-(ethylenedioxy)cyclohexane-1(e)-carbonitrile

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Chemical Property of trans-2(e),6(a)-diphenyl-4,4-(ethylenedioxy)cyclohexane-1(e)-carbonitrile

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Technology Process of trans-2(e),6(a)-diphenyl-4,4-(ethylenedioxy)cyclohexane-1(e)-carbonitrile

There total 5 articles about trans-2(e),6(a)-diphenyl-4,4-(ethylenedioxy)cyclohexane-1(e)-carbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 111904-74-6
methyl 1-cyano-trans-2(e),6(a)-diphenyl-4,4-(ethylenedioxy)cyclohexane-1(e)-carboxylate

: 111904-75-7
trans-2(e),6(a)-diphenyl-4,4-(ethylenedioxy)cyclohexane-1(e)-carbonitrile

Guidance literature:: With water; lithium chloride; In dimethyl sulfoxide; at 173 ℃; for 4h;
DOI:10.1021/jo00237a042

Reference yield: 78.0%

: 111904-73-5
ethyl 1-cyano-trans-2(e),6(a)-diphenyl-4,4-(ethylenedioxy)cyclohexane-1(e)-carboxylate

: 111904-75-7
trans-2(e),6(a)-diphenyl-4,4-(ethylenedioxy)cyclohexane-1(e)-carbonitrile

Guidance literature:: With water; lithium chloride; In dimethyl sulfoxide; at 147 - 170 ℃; for 4.5h;
DOI:10.1021/jo00237a042

Reference yield:

: 63087-40-1
1-cyano-trans-2,6-diphenyl-4-oxocyclohexane-1-carboxylate

: 111904-75-7
trans-2(e),6(a)-diphenyl-4,4-(ethylenedioxy)cyclohexane-1(e)-carbonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 69 percent / p-toluenesulfonic acid monohydrate / benzene / 3.3 h / Heating

2: 88 percent / LiCl, H₂O / dimethylsulfoxide / 4 h / 173 °C

With water; toluene-4-sulfonic acid; lithium chloride; In dimethyl sulfoxide; benzene;
DOI:10.1021/jo00237a042