p-trifluoroacetamidophenyl 4-O-α-D-glucopyranosyl-α-D-galactopyranoside

Base Information

Chemical Name:p-trifluoroacetamidophenyl 4-O-α-D-glucopyranosyl-α-D-galactopyranoside
CAS No.:85906-32-7
Molecular Formula:C₂₀H₂₆F₃NO₁₂
Molecular Weight:529.421
Hs Code.:

Synonyms:p-trifluoroacetamidophenyl 4-O-α-D-glucopyranosyl-α-D-galactopyranoside

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Chemical Property of p-trifluoroacetamidophenyl 4-O-α-D-glucopyranosyl-α-D-galactopyranoside

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Technology Process of p-trifluoroacetamidophenyl 4-O-α-D-glucopyranosyl-α-D-galactopyranoside

There total 8 articles about p-trifluoroacetamidophenyl 4-O-α-D-glucopyranosyl-α-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 85906-31-6
p-trifluoroacetamidophenyl 6-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-α-D-galactopyranoside

: 85906-32-7
p-trifluoroacetamidophenyl 4-O-α-D-glucopyranosyl-α-D-galactopyranoside

Guidance literature:: With hydrogen; palladium on activated charcoal; In acetic acid;
DOI:10.1016/0008-6215(83)88201-9

Reference yield:

: 25320-59-6
tetra-O-benzyl glucopyranosyl chloride

: 85906-32-7
p-trifluoroacetamidophenyl 4-O-α-D-glucopyranosyl-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 51 percent / silver triflate, 2,4,6-trimethylpyridine / toluene; CH₂Cl₂ / 0.25 h / Ambient temperature

2: 93 percent / sodium methoxide / methanol / Ambient temperature

3: 78 percent / hydrogen / 5 percent Pd/C / acetic acid

With 2,4,6-trimethyl-pyridine; hydrogen; sodium methylate; silver trifluoromethanesulfonate; palladium on activated charcoal; In methanol; dichloromethane; acetic acid; toluene;
DOI:10.1016/0008-6215(83)88201-9

Reference yield:

: 85906-28-1
p-nitrophenyl 2,3-di-O-acetyl-4,6-O-benzylidene-α-D-galactopyranoside

: 85906-32-7
p-trifluoroacetamidophenyl 4-O-α-D-glucopyranosyl-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) hydrogen / 1.) 5 percent Pd/C / 1.) ethyl acetate; 2.) pyridine, 30 min, r.t.

2: 76 percent / sodium cyanoborohydride, hydrogen chloride / tetrahydrofuran; diethyl ether

3: 51 percent / silver triflate, 2,4,6-trimethylpyridine / toluene; CH₂Cl₂ / 0.25 h / Ambient temperature

4: 93 percent / sodium methoxide / methanol / Ambient temperature

5: 78 percent / hydrogen / 5 percent Pd/C / acetic acid

With 2,4,6-trimethyl-pyridine; hydrogenchloride; hydrogen; sodium methylate; silver trifluoromethanesulfonate; sodium cyanoborohydride; palladium on activated charcoal; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; acetic acid; toluene;
DOI:10.1016/0008-6215(83)88201-9