di-tert-butyl N-<(4-phenyl)carbamoyl>-L-glutamate

Base Information

Chemical Name:di-tert-butyl N-<(4-phenyl)carbamoyl>-L-glutamate
CAS No.:161803-06-1
Molecular Formula:C₂₁H₃₂N₂O₆
Molecular Weight:408.495
Hs Code.:

di-tert-butyl N-<(4-<hydroxymethyl>phenyl)carbamoyl>-L-glutamate

Synonyms:di-tert-butyl N-<(4-phenyl)carbamoyl>-L-glutamate

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Chemical Property of di-tert-butyl N-<(4-phenyl)carbamoyl>-L-glutamate

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Technology Process of di-tert-butyl N-<(4-phenyl)carbamoyl>-L-glutamate

There total 7 articles about di-tert-butyl N-<(4-phenyl)carbamoyl>-L-glutamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 13.0%

: 161803-05-0
di-tert-butyl N-<(4-<oxymethyl>phenyl)carbamoyl>-L-glutamate

: tert-butyl 1-phenyl)carbamoyl>-5-oxopyrrolidine-2-carboxylate

: 161803-06-1
di-tert-butyl N-<(4-phenyl)carbamoyl>-L-glutamate

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; for 3h;
DOI:10.1021/jm980425k

Reference yield:

: 619-73-8
4-nitrobenzyl chloride

: 161803-06-1
di-tert-butyl N-<(4-phenyl)carbamoyl>-L-glutamate

Guidance literature:: Multi-step reaction with 5 steps

1: 93 percent / imidazole / dimethylformamide / 5 h / Ambient temperature

2: 91 percent / ammonium formate / 10 percent Pd/C / ethanol / 1.5 h / 20 °C

3: 99 percent / Et₃N / toluene / 5 h / 70 °C

4: 63 percent / Et₃N / tetrahydrofuran / 3 h / Ambient temperature

5: 58 percent / tetrabutylammonium fluoride / tetrahydrofuran / 3 h

With 1H-imidazole; tetrabutyl ammonium fluoride; ammonium formate; triethylamine; palladium on activated charcoal; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jm980425k

Reference yield:

: 161803-03-8
1-nitro-4-(tert-butyldiphenylsiloxymethyl)benzene

: 161803-06-1
di-tert-butyl N-<(4-phenyl)carbamoyl>-L-glutamate

Guidance literature:: Multi-step reaction with 4 steps

1: 91 percent / ammonium formate / 10 percent Pd/C / ethanol / 1.5 h / 20 °C

2: 99 percent / Et₃N / toluene / 5 h / 70 °C

3: 63 percent / Et₃N / tetrahydrofuran / 3 h / Ambient temperature

4: 58 percent / tetrabutylammonium fluoride / tetrahydrofuran / 3 h

With tetrabutyl ammonium fluoride; ammonium formate; triethylamine; palladium on activated charcoal; In tetrahydrofuran; ethanol; toluene;
DOI:10.1021/jm980425k