Phosphoric acid ethyl ester (1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentahydroxy-cyclohexyl ester

Base Information

Chemical Name:Phosphoric acid ethyl ester (1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentahydroxy-cyclohexyl ester
CAS No.:516497-78-2
Molecular Formula:C₈H₁₇O₉P
Molecular Weight:288.191
Hs Code.:

Synonyms:Phosphoric acid ethyl ester (1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentahydroxy-cyclohexyl ester

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Chemical Property of Phosphoric acid ethyl ester (1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentahydroxy-cyclohexyl ester

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Technology Process of Phosphoric acid ethyl ester (1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentahydroxy-cyclohexyl ester

There total 4 articles about Phosphoric acid ethyl ester (1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentahydroxy-cyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Phosphoric acid ethyl ester methyl ester (1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentakis-methoxymethoxy-cyclohexyl ester

: 516497-78-2
Phosphoric acid ethyl ester (1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentahydroxy-cyclohexyl ester

Guidance literature:: With 50percent aq. AcOH; at 50 - 60 ℃;
DOI:10.1021/ja029362s

Reference yield:

: 153996-50-0
1D-1-O-2,3,4,5,6-(pentakis)methoxymethylene-myo-inositol

: 516497-78-2
Phosphoric acid ethyl ester (1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentahydroxy-cyclohexyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: diisopropylethylamine / CHCl₃ / 6 h / -78 - 20 °C

2: CHCl₃ / 0 - 20 °C

3: t-BuOOH / decane

4: 50percent aq. AcOH / 50 - 60 °C

With tert.-butylhydroperoxide; N-ethyl-N,N-diisopropylamine; In decane; chloroform;
DOI:10.1021/ja029362s

Reference yield:

: Phosphorochloridous acid methyl ester (1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentakis-methoxymethoxy-cyclohexyl ester

: 516497-78-2
Phosphoric acid ethyl ester (1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentahydroxy-cyclohexyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: CHCl₃ / 0 - 20 °C

2: t-BuOOH / decane

3: 50percent aq. AcOH / 50 - 60 °C

With tert.-butylhydroperoxide; In decane; chloroform;
DOI:10.1021/ja029362s