tert-butyl 2-(tert-butoxycarbonylamino)-3-[4,5-methylenedioxy-2-(trifluoromethanesulfonyloxy)phenyl]-3-(3,4,5-trimethoxyphenyl)propanoate

Base Information

Chemical Name:tert-butyl 2-(tert-butoxycarbonylamino)-3-[4,5-methylenedioxy-2-(trifluoromethanesulfonyloxy)phenyl]-3-(3,4,5-trimethoxyphenyl)propanoate
CAS No.:1428470-85-2
Molecular Formula:C₂₉H₃₆F₃NO₁₂S
Molecular Weight:679.666
Hs Code.:

tert-butyl 2-(tert-butoxycarbonylamino)-3-[4,5-methylenedioxy-2-(trifluoromethanesulfonyloxy)phenyl]-3-(3,4,5-trimethoxyphenyl)propanoate

Synonyms:tert-butyl 2-(tert-butoxycarbonylamino)-3-[4,5-methylenedioxy-2-(trifluoromethanesulfonyloxy)phenyl]-3-(3,4,5-trimethoxyphenyl)propanoate

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Chemical Property of tert-butyl 2-(tert-butoxycarbonylamino)-3-[4,5-methylenedioxy-2-(trifluoromethanesulfonyloxy)phenyl]-3-(3,4,5-trimethoxyphenyl)propanoate

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Technology Process of tert-butyl 2-(tert-butoxycarbonylamino)-3-[4,5-methylenedioxy-2-(trifluoromethanesulfonyloxy)phenyl]-3-(3,4,5-trimethoxyphenyl)propanoate

There total 3 articles about tert-butyl 2-(tert-butoxycarbonylamino)-3-[4,5-methylenedioxy-2-(trifluoromethanesulfonyloxy)phenyl]-3-(3,4,5-trimethoxyphenyl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 1428470-83-0
tert-butyl 2-benzylamino-3-[4,5-methylenedioxy-2-(trifluoromethanesulfonyloxy)phenyl]-3-(3,4,5-trimethoxyphenyl)-propanoate

: 1428470-85-2
tert-butyl 2-(tert-butoxycarbonylamino)-3-[4,5-methylenedioxy-2-(trifluoromethanesulfonyloxy)phenyl]-3-(3,4,5-trimethoxyphenyl)propanoate

Guidance literature:: With palladium on activated charcoal; hydrogen; In ethyl acetate; at 20 ℃; for 6h;
DOI:10.1021/jo400147f

Reference yield:

: 533-31-3
Sesamol

: 1428470-85-2
tert-butyl 2-(tert-butoxycarbonylamino)-3-[4,5-methylenedioxy-2-(trifluoromethanesulfonyloxy)phenyl]-3-(3,4,5-trimethoxyphenyl)propanoate

Guidance literature:: Multi-step reaction with 3 steps

1: zinc trifluoromethanesulfonate / dichloromethane / 9 h / 30 °C

2: pyridine / dichloromethane / 5 h / 0 °C

3: palladium on activated charcoal; hydrogen / ethyl acetate / 6 h / 20 °C

With pyridine; palladium on activated charcoal; hydrogen; zinc trifluoromethanesulfonate; In dichloromethane; ethyl acetate;
DOI:10.1021/jo400147f

Reference yield:

: C₂₃H₂₉NO₅

: 1428470-85-2
tert-butyl 2-(tert-butoxycarbonylamino)-3-[4,5-methylenedioxy-2-(trifluoromethanesulfonyloxy)phenyl]-3-(3,4,5-trimethoxyphenyl)propanoate

Guidance literature:: Multi-step reaction with 3 steps

1: zinc trifluoromethanesulfonate / dichloromethane / 9 h / 30 °C

2: pyridine / dichloromethane / 5 h / 0 °C

3: palladium on activated charcoal; hydrogen / ethyl acetate / 6 h / 20 °C

With pyridine; palladium on activated charcoal; hydrogen; zinc trifluoromethanesulfonate; In dichloromethane; ethyl acetate;
DOI:10.1021/jo400147f