1-benzenesulfonyl-2-(3-methoxycarbonylmethyl-1H-indole-2-carbonyl)-1H-indole-3-carboxylic acid

Base Information

Chemical Name:1-benzenesulfonyl-2-(3-methoxycarbonylmethyl-1H-indole-2-carbonyl)-1H-indole-3-carboxylic acid
CAS No.:906565-30-8
Molecular Formula:C₂₇H₂₀N₂O₇S
Molecular Weight:516.531
Hs Code.:

1-benzenesulfonyl-2-(3-methoxycarbonylmethyl-1<i>H</i>-indole-2-carbonyl)-1<i>H</i>-indole-3-carboxylic acid

Synonyms:1-benzenesulfonyl-2-(3-methoxycarbonylmethyl-1H-indole-2-carbonyl)-1H-indole-3-carboxylic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-benzenesulfonyl-2-(3-methoxycarbonylmethyl-1H-indole-2-carbonyl)-1H-indole-3-carboxylic acid

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Technology Process of 1-benzenesulfonyl-2-(3-methoxycarbonylmethyl-1H-indole-2-carbonyl)-1H-indole-3-carboxylic acid

There total 1 articles about 1-benzenesulfonyl-2-(3-methoxycarbonylmethyl-1H-indole-2-carbonyl)-1H-indole-3-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1912-33-0
Indole-3-acetic acid methyl ester

: 192991-42-7
1-(benzenesulfonyl)indole-2,3-dicarboxylic anhydride

: 906565-30-8
1-benzenesulfonyl-2-(3-methoxycarbonylmethyl-1H-indole-2-carbonyl)-1H-indole-3-carboxylic acid

Guidance literature:: With titanium tetrachloride; In dichloromethane;
DOI:10.1016/j.tetlet.2006.04.157

Reference yield:

: 906565-30-8
1-benzenesulfonyl-2-(3-methoxycarbonylmethyl-1H-indole-2-carbonyl)-1H-indole-3-carboxylic acid

: 906565-32-0
[1-benzyl-2-(1-benzyl-1H-indole-2-carbonyl)-1H-indol-3-yl]-acetic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: KOH / H₂O / Heating

1.2: 41 percent / H₂SO₄

2.1: 100 percent / K₂CO₃ / acetonitrile / Heating

With potassium hydroxide; potassium carbonate; In water; acetonitrile;
DOI:10.1016/j.tetlet.2006.04.157

Reference yield:

: 906565-30-8
1-benzenesulfonyl-2-(3-methoxycarbonylmethyl-1H-indole-2-carbonyl)-1H-indole-3-carboxylic acid

: C₃₅H₂₆N₂O₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: KOH / H₂O / Heating

1.2: 41 percent / H₂SO₄

2.1: 100 percent / K₂CO₃ / acetonitrile / Heating

3.1: 59 percent / POCl₃

4.1: 64 percent / NaH / tetrahydrofuran

With potassium hydroxide; sodium hydride; potassium carbonate; trichlorophosphate; In tetrahydrofuran; water; acetonitrile;
DOI:10.1016/j.tetlet.2006.04.157