Technology Process of C25H39NO6S
There total 1 articles about C25H39NO6S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C16H25NO4S;
With
sodium hydride;
In
tetrahydrofuran; mineral oil;
at 0 ℃;
for 0.25h;
Inert atmosphere;
(Z)-4-[(tetrahydropyran-2-yl)oxy]-2-buten-1-yl bromide;
In
tetrahydrofuran; mineral oil;
for 16h;
Inert atmosphere;
Reflux;
DOI:10.1002/chem.201002606
- Guidance literature:
-
With
hydrogenchloride;
In
tetrahydrofuran; water;
at 80 ℃;
for 24h;
DOI:10.1002/chem.201002606
- Guidance literature:
-
Multi-step reaction with 2 steps
1: hydrogenchloride / tetrahydrofuran; water / 24 h / 80 °C
2: (R)-((4,4’-bi-1,3-benzodioxole)-5,5’-diyl)bis(bis(3,5-di-t-butyl-4-methoxyphenyl))phosphine; dimethylsulfide gold(I) chloride; silver(I) triflimide / dichloromethane; toluene / 4 h / -10 °C / Inert atmosphere; Darkness
With
(R)-((4,4’-bi-1,3-benzodioxole)-5,5’-diyl)bis(bis(3,5-di-t-butyl-4-methoxyphenyl))phosphine; hydrogenchloride; dimethylsulfide gold(I) chloride; silver(I) triflimide;
In
tetrahydrofuran; dichloromethane; water; toluene;
DOI:10.1002/chem.201002606