Technology Process of 1,3-Bis(trifluoromethylsulfonyl)-5-nitro-2,4,6-trichlorobenzene
There total 3 articles about 1,3-Bis(trifluoromethylsulfonyl)-5-nitro-2,4,6-trichlorobenzene which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
chromium(VI) oxide; sulfuric acid;
In
acetic acid;
1)25 deg C, 30 min.;2)60 deg C, 30 min.;3)75-80 deg C, 1h.;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 94 percent / conc. HCl, 30percent H2O2 / acetic acid / 10 - 13 °C
2: 78 percent / Trifluoroacetic anhydride, 90percentH2O2 / 0.67 h / -20 °C
3: 92 percent / conc. H2SO4, CrO3 / acetic acid / 1)25 deg C, 30 min.;2)60 deg C, 30 min.;3)75-80 deg C, 1h.
With
chromium(VI) oxide; hydrogenchloride; sulfuric acid; dihydrogen peroxide; trifluoroacetic anhydride;
In
acetic acid;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 78 percent / Trifluoroacetic anhydride, 90percentH2O2 / 0.67 h / -20 °C
2: 92 percent / conc. H2SO4, CrO3 / acetic acid / 1)25 deg C, 30 min.;2)60 deg C, 30 min.;3)75-80 deg C, 1h.
With
chromium(VI) oxide; sulfuric acid; dihydrogen peroxide; trifluoroacetic anhydride;
In
acetic acid;
