{Os(C₆H₆)(P(CH(CH₃)2)3)(NC(C₆H₅)2)}⁽¹⁺⁾*PF₆^(1-)={Os(C₆H₆)(P(CH(CH₃)2)3)(NC(C₆H₅)2)}PF₆

Base Information

• Chemical Name: {Os(C₆H₆)(P(CH(CH₃)2)3)(NC(C₆H₅)2)}⁽¹⁺⁾*PF₆^(1-)={Os(C₆H₆)(P(CH(CH₃)2)3)(NC(C₆H₅)2)}PF₆
• CAS No.: 135455-18-4
• Molecular Formula: C₂₈H₃₇NOsP*F₆P
• Molecular Weight: 753.746

Synonyms:{Os(C₆H₆)(P(CH(CH₃)2)3)(NC(C₆H₅)2)}⁽¹⁺⁾*PF₆^(1-)={Os(C₆H₆)(P(CH(CH₃)2)3)(NC(C₆H₅)2)}PF₆

Chemical Property of {Os(C₆H₆)(P(CH(CH₃)2)3)(NC(C₆H₅)2)}⁽¹⁺⁾*PF₆^(1-)={Os(C₆H₆)(P(CH(CH₃)2)3)(NC(C₆H₅)2)}PF₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of {Os(C₆H₆)(P(CH(CH₃)2)3)(NC(C₆H₅)2)}⁽¹⁺⁾*PF₆^(1-)={Os(C₆H₆)(P(CH(CH₃)2)3)(NC(C₆H₅)2)}PF₆

There total 3 articles about {Os(C₆H₆)(P(CH(CH₃)2)3)(NC(C₆H₅)2)}⁽¹⁺⁾*PF₆^(1-)={Os(C₆H₆)(P(CH(CH₃)2)3)(NC(C₆H₅)2)}PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

{OsI(C6H6)(P(CH(CH3)2)3)(NHC(C6H5)2)}(1+)*PF6(1-)={OsI(C6H6)(P(CH(CH3)2)3)(NHC(C6H5)2)}PF6 (135455-16-2) → {Os(C6H6)(P(CH(CH3)2)3)(NC(C6H5)2)}(1+)*PF6(1-)={Os(C6H6)(P(CH(CH3)2)3)(NC(C6H5)2)}PF6 (135455-18-4)

Guidance literature:

With N(C₂H₅)3; In dichloromethane; byproducts: HI; under Ar, stirred for 15 min at room temp.; removal of solvent in vac., dissolved in CH2Cl2, chromy. (Al2O3, CH2Cl2), evapn. to dryness, recrystn. (CH2Cl2/ether);

Reference yield: 86.0%

potassium hexafluorophosphate (17084-13-8) + Benzophenone imine (1013-88-3) + (η6-C6H6)OsI2(P-i-Pr3) (97477-25-3) → {Os(C6H6)(P(CH(CH3)2)3)(NC(C6H5)2)}(1+)*PF6(1-)={Os(C6H6)(P(CH(CH3)2)3)(NC(C6H5)2)}PF6 (135455-18-4)

Guidance literature:

In methanol; under Ar, stirred for 30 min at room temp.; removal of solvent in vac., extn. (CH2Cl2), evapn., chromy. (Al2O3, CH2Cl2), evapn. to dryness in vac., recrystn. (CH2Cl2/ether); elem. anal.;

Reference yield: 58.0%

ammonium hexafluorophosphate + (η6-C6H6)OsI2(P-i-Pr3) (97477-25-3) + diphenylmethyleneimino lithium (19112-47-1) → {Os(C6H6)(P(CH(CH3)2)3)(NC(C6H5)2)}(1+)*PF6(1-)={Os(C6H6)(P(CH(CH3)2)3)(NC(C6H5)2)}PF6 (135455-18-4)

Guidance literature:

In diethyl ether; toluene; under Ar, dropwise addn. of LiNCPh2 in ether to Os-compd. in toluene, stirred for 30 min at room temp.; removal of solvent in vac., addn. of NH4PF6 in methanol, stirred for 20 min at room temp., extn. (CH2Cl2), evapn. in vac., recrystn. (CH2Cl2/ether); elem. anal.;

upstream raw materials:

(η6-C6H6)OsI2(P-i-Pr3)

diphenylmethyleneimino lithium

potassium hexafluorophosphate

Benzophenone imine

Downstream raw materials:

{C₆H₆OsH(NHC(C₆H₅)2)(P(CH(CH₃)2)3)}⁽¹⁺⁾*PF₆^(1-)={C₆H₆HOs(NHC(C₆H₅)2)(P(CH(CH₃)2)3)}PF₆

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 135455-18-4 {Os(C₆H₆)(P(CH(CH₃)2)3)(NC(C₆H₅)2)}⁽¹⁺⁾*PF₆^(1-)={Os(C₆H₆)(P(CH(CH₃)2)3)(NC(C₆H₅)2)}PF₆

Send

Send

Metric Ton KG G Pound L ML

Send

Send