Bicyclo[2.2.1]hept-5-ene-2-carboxaldehyde, 3-ethyl-, (2-endo,3-exo)- (9CI)

Base Information

Chemical Name:Bicyclo[2.2.1]hept-5-ene-2-carboxaldehyde, 3-ethyl-, (2-endo,3-exo)- (9CI)
CAS No.:136655-70-4
Molecular Formula:C10H14O
Molecular Weight:150.22
Hs Code.:
Mol file:136655-70-4.mol

Synonyms:Bicyclo[2.2.1]hept-5-ene-2-carboxaldehyde, 3-ethyl-, (2-endo,3-exo)- (9CI)

Suppliers and Price of Bicyclo[2.2.1]hept-5-ene-2-carboxaldehyde, 3-ethyl-, (2-endo,3-exo)- (9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Bicyclo[2.2.1]hept-5-ene-2-carboxaldehyde, 3-ethyl-, (2-endo,3-exo)- (9CI)

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of Bicyclo[2.2.1]hept-5-ene-2-carboxaldehyde, 3-ethyl-, (2-endo,3-exo)- (9CI)

There total 14 articles about Bicyclo[2.2.1]hept-5-ene-2-carboxaldehyde, 3-ethyl-, (2-endo,3-exo)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1576-87-0
trans-2-pentenal

: 542-92-7,25568-84-7,7313-32-8
cyclopenta-1,3-diene

: 77-73-6,933-60-8,1755-01-7,25038-78-2
bi(cyclopentadiene)

: 136559-32-5,136655-70-4
C₁₀H₁₄O

Guidance literature:: With (R,R)-N,N-bis(3,5-di-tert-butylsalicylidene)-1,2-cyclohexanediaminochromium(III) chloride; sodium dodecyl-sulfate; In water; at 25 ℃; for 20h;
DOI:10.1016/j.tetlet.2011.10.088

Reference yield:

: 1576-87-0
trans-2-pentenal

: 542-92-7,25568-84-7,7313-32-8
cyclopenta-1,3-diene

: 136655-70-4
(1S,2R,3R,4R)-3-Ethyl-bicyclo[2.2.1]hept-5-ene-2-carbaldehyde

: 136655-70-4
(1R,2R,3R,4S)-3-Ethyl-bicyclo[2.2.1]hept-5-ene-2-carbaldehyde

Guidance literature:: With (R)-3-(2-hydroxy-3-phenylphenyl)-2,2'-dihydroxy-1,1'-binaphthyl*3,5-bis(trifluoromethyl)benzeneboronic acid; In dichloromethane; at -78 ℃; for 72h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1021/ja9810282

Reference yield:

: 1576-87-0
trans-2-pentenal

: 542-92-7,25568-84-7,7313-32-8
cyclopenta-1,3-diene

: 136655-70-4
(1S,2R,3R,4R)-3-Ethyl-bicyclo[2.2.1]hept-5-ene-2-carbaldehyde

: 136655-70-4
(1R,2R,3R,4S)-3-Ethyl-bicyclo[2.2.1]hept-5-ene-2-carbaldehyde

Guidance literature:: With (R)-3-(2-hydroxy-3-phenylphenyl)-2,2'-dihydroxy-1,1'-binaphthyl*3,5-bis(trifluoromethyl)benzeneboronic acid; In dichloromethane; at -78 ℃; for 72h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1021/ja9810282