(O-methyl phenylphosphinito)chlorodicarbonylbis(triphenylphosphine)osmium(II)

Base Information

Chemical Name:(O-methyl phenylphosphinito)chlorodicarbonylbis(triphenylphosphine)osmium(II)
CAS No.:102781-85-1
Molecular Formula:C₄₅H₃₈ClO₃OsP₃
Molecular Weight:945.369
Hs Code.:

Synonyms:(O-methyl phenylphosphinito)chlorodicarbonylbis(triphenylphosphine)osmium(II)

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Chemical Property of (O-methyl phenylphosphinito)chlorodicarbonylbis(triphenylphosphine)osmium(II)

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Technology Process of (O-methyl phenylphosphinito)chlorodicarbonylbis(triphenylphosphine)osmium(II)

There total 2 articles about (O-methyl phenylphosphinito)chlorodicarbonylbis(triphenylphosphine)osmium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 94780-65-1
chloro(O-methyl phenylphosphinite)dicarbonylbis(triphenylphosphine)osmium(II) hexafluoroantimonate

: 102781-85-1
(O-methyl phenylphosphinito)chlorodicarbonylbis(triphenylphosphine)osmium(II)

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In benzene; byproducts: DBU*HSbF6; N2 atmosphere; addn. of DBU to suspn. of Os-complex; stirring for 5 min;; sepn. of oily DBU*HSbF6; cooling in ice; crystn. on addn. of hexane; filtration; washing (hexane, MeOH, EtOH); recrystn. (benzene/hexane);