alpha-D-arabino-Heptopyranosidurononitrile, ethyl 2,6-dideoxy- (9CI)

Base Information

Chemical Name:alpha-D-arabino-Heptopyranosidurononitrile, ethyl 2,6-dideoxy- (9CI)
CAS No.:148379-96-8
Molecular Formula:C₉H₁₅NO₄
Molecular Weight:201.222
Hs Code.:
Mol file:148379-96-8.mol

Synonyms:alpha-D-arabino-Heptopyranosidurononitrile, ethyl 2,6-dideoxy- (9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of alpha-D-arabino-Heptopyranosidurononitrile, ethyl 2,6-dideoxy- (9CI)

Chemical Property:

Purity/Quality:

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Technology Process of alpha-D-arabino-Heptopyranosidurononitrile, ethyl 2,6-dideoxy- (9CI)

There total 7 articles about alpha-D-arabino-Heptopyranosidurononitrile, ethyl 2,6-dideoxy- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 148379-94-6
Ethyl 3,4-di-O-acetyl-2,6-dideoxy-α-D-arabino-heptopyranurononitrile

: 148379-96-8
Ethyl 2,6-dideoxy-α-D-arabino-heptopyranurononitrile

Guidance literature:: With sodium methylate; In methanol; Ambient temperature;
DOI:10.1021/jo00063a048

Reference yield:

: 63069-75-0
ethyl 3,4,6-tri-O-acetyl-2-deoxy-α-D-arabino-hexopyranoside

: 148379-96-8
Ethyl 2,6-dideoxy-α-D-arabino-heptopyranurononitrile

Guidance literature:: Multi-step reaction with 7 steps

1: NaOMe / methanol / Ambient temperature

2: pyridine / Ambient temperature

3: pyridine / Ambient temperature

4: BF₃*Et₂O / ethanol; CH₂Cl₂ / Ambient temperature

5: pyridine / CH₂Cl₂ / 0.08 h / 0 °C

6: acetonitrile / 0.08 h

7: 95 percent / NaOMe / methanol / Ambient temperature

With pyridine; boron trifluoride diethyl etherate; sodium methylate; In methanol; ethanol; dichloromethane; acetonitrile;
DOI:10.1021/jo00063a048

Reference yield:

: 148379-92-4
Ethyl 3,4-di-O-acetyl-2-deoxy-α-D-arabino-hexopyranoside

: 148379-96-8
Ethyl 2,6-dideoxy-α-D-arabino-heptopyranurononitrile

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / CH₂Cl₂ / 0.08 h / 0 °C

2: acetonitrile / 0.08 h

3: 95 percent / NaOMe / methanol / Ambient temperature

With pyridine; sodium methylate; In methanol; dichloromethane; acetonitrile;
DOI:10.1021/jo00063a048