dibenzo-4,5,6,7 (dimethylaminomethyl-2 phenyl)-2 phenyl-2 dioxasilacycloheptadiene-1,3,2

Base Information

Chemical Name:dibenzo-4,5,6,7 (dimethylaminomethyl-2 phenyl)-2 phenyl-2 dioxasilacycloheptadiene-1,3,2
CAS No.:133156-72-6
Molecular Formula:C₂₇H₂₅NO₂Si
Molecular Weight:423.587
Hs Code.:

Synonyms:dibenzo-4,5,6,7 (dimethylaminomethyl-2 phenyl)-2 phenyl-2 dioxasilacycloheptadiene-1,3,2

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Chemical Property of dibenzo-4,5,6,7 (dimethylaminomethyl-2 phenyl)-2 phenyl-2 dioxasilacycloheptadiene-1,3,2

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Technology Process of dibenzo-4,5,6,7 (dimethylaminomethyl-2 phenyl)-2 phenyl-2 dioxasilacycloheptadiene-1,3,2

There total 3 articles about dibenzo-4,5,6,7 (dimethylaminomethyl-2 phenyl)-2 phenyl-2 dioxasilacycloheptadiene-1,3,2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1806-29-7
2,2'-dihydroxybiphenyl

: 114499-75-1
(dimethylaminomethyl-2 phenyl)-1 phenylsilane

: 133156-72-6
dibenzo-4,5,6,7 (dimethylaminomethyl-2 phenyl)-2 phenyl-2 dioxasilacycloheptadiene-1,3,2

Guidance literature:: In tetrachloromethane; at 25 ℃; for 5h;
DOI:10.1016/0022-328X(90)80080-J

Reference yield:

: 103-83-3
N,N'-dimethylbenzylamine

: 133156-72-6
dibenzo-4,5,6,7 (dimethylaminomethyl-2 phenyl)-2 phenyl-2 dioxasilacycloheptadiene-1,3,2

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-BuLi / 1.) Et₂O, hexane, rt, 48 h, 2.) rt, 48 h

2: 76 percent / CCl₄ / 5 h / 25 °C

With n-butyllithium; In tetrachloromethane;
DOI:10.1016/0022-328X(90)80080-J

Reference yield:

: 694-53-1
phenylsilane

: 133156-72-6
dibenzo-4,5,6,7 (dimethylaminomethyl-2 phenyl)-2 phenyl-2 dioxasilacycloheptadiene-1,3,2

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-BuLi / 1.) Et₂O, hexane, rt, 48 h, 2.) rt, 48 h

2: 76 percent / CCl₄ / 5 h / 25 °C

With n-butyllithium; In tetrachloromethane;
DOI:10.1016/0022-328X(90)80080-J