C₂₉H₂₃NO₆

Base Information

• Chemical Name: C₂₉H₂₃NO₆
• CAS No.: 141328-75-8
• Molecular Formula: C₂₉H₂₃NO₆
• Molecular Weight: 481.505
• Mol file: 141328-75-8.mol

Synonyms:C₂₉H₂₃NO₆

Chemical Property of C₂₉H₂₃NO₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₉H₂₃NO₆

There total 1 articles about C₂₉H₂₃NO₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

C26H19NO4 (130031-63-9) + bromoacetic acid methyl ester (96-32-2) → C29H23NO6 (141328-75-8)

Guidance literature:

With 18-crown-6 ether; caesium carbonate; In acetonitrile; for 10h; Ambient temperature;

DOI:10.1021/ja00049a022

Reference yield:

C29H23NO6 (141328-75-8) → C28H21NO6 (141328-76-9)

Guidance literature:

With lithium hydroxide; In tetrahydrofuran; at 0 ℃; for 0.5h;

DOI:10.1021/ja00049a022

Reference yield:

C29H23NO6 (141328-75-8) → C28H23NO5 (132938-56-8)

Guidance literature:

Multi-step reaction with 3 steps

1: 0.5 N aq. LiOH / tetrahydrofuran / 0.5 h / 0 °C

2: triphenylphosphine / CH₂Cl₂ / 0.5 h / 0 °C

3: 68 percent / sodium borohydride / CH₂Cl₂; propan-2-ol / 0.5 h / 0 °C

With lithium hydroxide; sodium tetrahydroborate; triphenylphosphine; In tetrahydrofuran; dichloromethane; isopropyl alcohol;

DOI:10.1021/ja00049a022

upstream raw materials:

C₂₆H₁₉NO₄

bromoacetic acid methyl ester

Downstream raw materials:

C₂₈H₂₁NO₆

C₂₈H₂₃NO₅

C₃₃H₂₄N₂O₅S

C₃₀H₂₇NO₇S