1-[2-(4-Bromo-phenyl)-2-oxo-ethyl]-3-methyl-3H-tetrazol-1-ium; bromide

Base Information

• Chemical Name: 1-[2-(4-Bromo-phenyl)-2-oxo-ethyl]-3-methyl-3H-tetrazol-1-ium; bromide
• CAS No.: 107403-53-2
• Molecular Formula: Br*C₁₀H₁₀BrN₄O
• Molecular Weight: 362.024
• Mol file: 107403-53-2.mol

Synonyms:1-[2-(4-Bromo-phenyl)-2-oxo-ethyl]-3-methyl-3H-tetrazol-1-ium; bromide

Chemical Property of 1-[2-(4-Bromo-phenyl)-2-oxo-ethyl]-3-methyl-3H-tetrazol-1-ium; bromide

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 1-[2-(4-Bromo-phenyl)-2-oxo-ethyl]-3-methyl-3H-tetrazol-1-ium; bromide

There total 1 articles about 1-[2-(4-Bromo-phenyl)-2-oxo-ethyl]-3-methyl-3H-tetrazol-1-ium; bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

2-methyltetrazole (16681-78-0,94848-54-1) + para-bromophenacyl bromide (99-73-0,132309-76-3) → 1-[2-(4-Bromo-phenyl)-2-oxo-ethyl]-3-methyl-3H-tetrazol-1-ium; bromide (107403-53-2)

Guidance literature:

With silver tetrafluoroborate; anion exchange resin/Br; In nitromethane; at 50 - 60 ℃; for 48h;

Reference yield: 96.0%

1-[2-(4-Bromo-phenyl)-2-oxo-ethyl]-3-methyl-3H-tetrazol-1-ium; bromide (107403-53-2) → 2C10H9BrN4O*H2O

Guidance literature:

With potassium carbonate; In water; at 0 ℃; for 2h;

Reference yield:

1-[2-(4-Bromo-phenyl)-2-oxo-ethyl]-3-methyl-3H-tetrazol-1-ium; bromide (107403-53-2) → 2-bromo-1-(4-bromophenyl)-3-phenyl-1-propanone (59824-91-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 96 percent / potassium carbonate / H₂O / 2 h / 0 °C

2: 16 percent / dimethylformamide / 120 h

With potassium carbonate; In water; N,N-dimethyl-formamide;

upstream raw materials:

2-methyltetrazole

para-bromophenacyl bromide

Downstream raw materials:

2-bromo-1-(4-bromophenyl)-3-phenyl-1-propanone