C₃₇H₃₄N₂O₄

Base Information

• Chemical Name: C₃₇H₃₄N₂O₄
• CAS No.: 1448026-25-2
• Molecular Formula: C₃₇H₃₄N₂O₄
• Molecular Weight: 570.688

Synonyms:C₃₇H₃₄N₂O₄

Chemical Property of C₃₇H₃₄N₂O₄

Chemical Property:

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Technology Process of C₃₇H₃₄N₂O₄

There total 8 articles about C₃₇H₃₄N₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

C37H36N2O4 → C37H34N2O4 (1448026-25-2)

Guidance literature:

C₃₇H₃₆N₂O₄; With sodium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 0.5h;

With iodine; In tetrahydrofuran; at -78 - 20 ℃; Solvent; Reagent/catalyst; Temperature;

DOI:10.1016/j.tetlet.2013.05.146

Reference yield:

C37H36N2O4 → C37H34N2O4 (1448026-25-2) + C37H34N2O4 (1448026-29-6) + C37H34N2O4 (616890-10-9)

Guidance literature:

C₃₇H₃₆N₂O₄; With lithium diisopropyl amide; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; at -78 ℃; for 0.5h;

With iodine; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; at -78 - 20 ℃; for 0.5h; Overall yield = 68 %; diastereoselective reaction;

DOI:10.1016/j.tetlet.2013.05.146

Reference yield:

C22H23NO4 → C37H34N2O4 (1448026-25-2)

Guidance literature:

Multi-step reaction with 4 steps

1.1: N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium / hexane; tetrahydrofuran / 1 h / -78 °C

1.2: 1 h / -78 °C

2.1: methanesulfonyl chloride; triethylamine / dichloromethane / 4 h / -60 - 0 °C

3.1: hydrogen / methanol / 2 h / 760.05 Torr

4.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C

4.2: -78 - 20 °C

With N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; hydrogen; sodium hexamethyldisilazane; methanesulfonyl chloride; triethylamine; In tetrahydrofuran; methanol; hexane; dichloromethane; 1.2: |Aldol Condensation;

DOI:10.1016/j.tetlet.2013.05.146

Downstream raw materials:

C₃₄H₃₀N₂O₄

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