Dimethyl 2-<3-<2-b,N^b-bis(phenylmethyl)amino>ethyl>indolyl>propanedioate

Base Information

• Chemical Name: Dimethyl 2-<3-<2-b,N^b-bis(phenylmethyl)amino>ethyl>indolyl>propanedioate
• CAS No.: 153275-89-9
• Molecular Formula: C₂₉H₃₀N₂O₄
• Molecular Weight: 470.568

Synonyms:Dimethyl 2-<3-<2-b,N^b-bis(phenylmethyl)amino>ethyl>indolyl>propanedioate

Chemical Property of Dimethyl 2-<3-<2-b,N^b-bis(phenylmethyl)amino>ethyl>indolyl>propanedioate

Chemical Property:

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Technology Process of Dimethyl 2-<3-<2-b,N^b-bis(phenylmethyl)amino>ethyl>indolyl>propanedioate

There total 1 articles about Dimethyl 2-<3-<2-b,N^b-bis(phenylmethyl)amino>ethyl>indolyl>propanedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Thallium dimethyl malonate + Dibenzyl-[2-(3-chloro-3H-indol-3-yl)-ethyl]-amine (153275-88-8) → Dimethyl 2-<3-<2-b,Nb-bis(phenylmethyl)amino>ethyl>indolyl>propanedioate (153275-89-9)

Guidance literature:

In tetrahydrofuran; Yield given; 1.) -78 deg C, 1 h, 2.) 23 deg C, 12 h;

DOI:10.1021/jo00078a029

Reference yield: 84.0%

Dimethyl 2-<3-<2-b,Nb-bis(phenylmethyl)amino>ethyl>indolyl>propanedioate (153275-89-9) → Methyl 3-<2-b,Nb-bis(phenylmethyl)amino>ethyl>indole-2-ethanoate (146681-76-7)

Guidance literature:

With triethylamine hydrochloride; lithium chloride; In N,N-dimethyl acetamide; at 130 ℃; for 2.5h;

DOI:10.1021/jo00078a029

Reference yield: 84.0%

Dimethyl 2-<3-<2-b,Nb-bis(phenylmethyl)amino>ethyl>indolyl>propanedioate (153275-89-9) → Dimethyl 2-<3-<2-b-(phenylmethyl)amino>ethyl>indolyl>propanedioate (153275-90-2)

Guidance literature:

With hydrogen; palladium on activated charcoal; In acetic acid;

DOI:10.1021/jo00078a029

upstream raw materials:

Dibenzyl-[2-(3-chloro-3H-indol-3-yl)-ethyl]-amine

Downstream raw materials:

Methyl 3-<2-b,N^b-bis(phenylmethyl)amino>ethyl>indole-2-ethanoate

Dimethyl 2-<3-<2-b-(phenylmethyl)amino>ethyl>indolyl>propanedioate

2-<(methoxycarbonyl)methyl>-3-<2-(N^b-benzylamino)ethyl>indole

Methyl 2-<2'-<3'-furanyl>-1'-(N_b-phenylmethyl)spiro<3H-indole-3,3'-pyrrolidin>-2(1H)-ylidene>acetate

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