C₃₀H₃₀F₅N₃O₅S

Base Information

Chemical Name:C₃₀H₃₀F₅N₃O₅S
CAS No.:1560643-26-6
Molecular Formula:C₃₀H₃₀F₅N₃O₅S
Molecular Weight:639.643
Hs Code.:

C<sub>30</sub>H<sub>30</sub>F<sub>5</sub>N<sub>3</sub>O<sub>5</sub>S

Synonyms:C₃₀H₃₀F₅N₃O₅S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₀H₃₀F₅N₃O₅S

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Technology Process of C₃₀H₃₀F₅N₃O₅S

There total 13 articles about C₃₀H₃₀F₅N₃O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1007882-13-4
(S)-tert-butyl 4,4-difluoro-2-(5-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-1H-imidazol-2-yl)pyrrolidine-1-carboxylate

: 1401068-73-2
C₁₃H₁₀F₆O₆S₂

: 1560643-26-6
C₃₀H₃₀F₅N₃O₅S

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In 1,2-dimethoxyethane; water; at 90 ℃; for 2h;

Reference yield:

: 203866-15-3
1-(tert-butoxycarbonyl)-4,4-difluoro-L-proline

: 1560643-26-6
C₃₀H₃₀F₅N₃O₅S

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / dichloromethane / 3 h / 20 °C

2: ammonium acetate / toluene / 5 h / 110 °C

3: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate / 1,2-dimethoxyethane / 2 h / 90 °C / Inert atmosphere

4: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / 1,2-dimethoxyethane; water / 2 h / 90 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; ammonium acetate; potassium acetate; potassium carbonate; triethylamine; In 1,2-dimethoxyethane; dichloromethane; water; toluene;

Reference yield:

: 74844-91-0,114676-69-6,135042-17-0,227935-38-8,102195-79-9
(2S,4S)-N-tert-butoxycarbonyl-4-hydroxyproline methyl ester

: 1560643-26-6
C₃₀H₃₀F₅N₃O₅S

Guidance literature:: Multi-step reaction with 7 steps

1.1: Dess-Martin periodane / dichloromethane / 7 h / 0 - 20 °C

2.1: diethylamino-sulfur trifluoride / dichloromethane / 21 h / -78 - 20 °C

3.1: lithium hydroxide; water / tetrahydrofuran / 2 h / 0 - 20 °C

3.2: pH 2

4.1: triethylamine / dichloromethane / 3 h / 20 °C

5.1: ammonium acetate / toluene / 5 h / 110 °C

6.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate / 1,2-dimethoxyethane / 2 h / 90 °C / Inert atmosphere

7.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / 1,2-dimethoxyethane; water / 2 h / 90 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; diethylamino-sulfur trifluoride; ammonium acetate; water; potassium acetate; potassium carbonate; Dess-Martin periodane; triethylamine; lithium hydroxide; In tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; water; toluene;