(1S,2S,5S)-(+)-6,6-dimethylbicyclo[3.1.1]heptan-2-yl dimethylphenylsilyl ketone

Base Information

• Chemical Name: (1S,2S,5S)-(+)-6,6-dimethylbicyclo[3.1.1]heptan-2-yl dimethylphenylsilyl ketone
• CAS No.: 150614-93-0
• Molecular Formula: C₁₈H₂₆OSi
• Molecular Weight: 286.489

Synonyms:(1S,2S,5S)-(+)-6,6-dimethylbicyclo[3.1.1]heptan-2-yl dimethylphenylsilyl ketone

Chemical Property of (1S,2S,5S)-(+)-6,6-dimethylbicyclo[3.1.1]heptan-2-yl dimethylphenylsilyl ketone

Chemical Property:

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Technology Process of (1S,2S,5S)-(+)-6,6-dimethylbicyclo[3.1.1]heptan-2-yl dimethylphenylsilyl ketone

There total 2 articles about (1S,2S,5S)-(+)-6,6-dimethylbicyclo[3.1.1]heptan-2-yl dimethylphenylsilyl ketone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(1S,2R,5S)-(-)-6,6-dimethylbicyclo<3.1.1>heptan-2-yl dimethylphenylsilyl ketone (150614-94-1) → (1S,2R,5S)-6,6-dimethylbicyclo[3.1.1]heptane-2-carbaldehyde (140225-13-4) + (1S,2S,5S)-(+)-6,6-dimethylbicyclo[3.1.1]heptane-2-carboxaldehyde (128301-02-0) + (1S,2S,5S)-(+)-6,6-dimethylbicyclo[3.1.1]heptan-2-yl dimethylphenylsilyl ketone (150614-93-0)

Guidance literature:

With hydrogenchloride; In diethyl ether; at 0 ℃; for 0.5h;

Reference yield:

myrtanyl chloride (108318-82-7,150614-86-1) → (1S,2S,5S)-(+)-6,6-dimethylbicyclo[3.1.1]heptan-2-yl dimethylphenylsilyl ketone (150614-93-0)

Guidance literature:

In tetrahydrofuran; Yield given; 1.) -78 deg C, 1 h, 2.) 0 deg C, 30 min;

Reference yield: 77.0%

(1S,2S,5S)-(+)-6,6-dimethylbicyclo[3.1.1]heptan-2-yl dimethylphenylsilyl ketone (150614-93-0) → (1S,2S,5S)-(-)-6,6-dimethylbicyclo<3.1.1>heptan-2-yl dimethylphenylsilyl thioketone (150615-00-2)

Guidance literature:

With hydrogenchloride; hydrogen sulfide; In diethyl ether; at -30 ℃;

upstream raw materials:

(1S,2R,5S)-(-)-6,6-dimethylbicyclo<3.1.1>heptan-2-yl dimethylphenylsilyl ketone

myrtanyl chloride

Downstream raw materials:

(1S,2S,5S)-(-)-6,6-dimethylbicyclo<3.1.1>heptan-2-yl dimethylphenylsilyl thioketone

(S)-1-((1S,2S,5S)-6,6-Dimethyl-bicyclo[3.1.1]hept-2-yl)-1-(dimethyl-phenyl-silanyl)-but-3-en-1-ol

(E)-(1S,2S,5S)-(-)-6,6-dimethylbicyclo<3.1.1>heptan-2-yl dimethylphenylsilyl thioketone S-oxide

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