2-<2-Nitro-3.4.5-trimethoxyphenyl>-3'-methoxy-propiophenon

Base Information

Chemical Name:2-<2-Nitro-3.4.5-trimethoxyphenyl>-3'-methoxy-propiophenon
CAS No.:109158-32-9
Molecular Formula:C₁₉H₂₁NO₇
Molecular Weight:375.378
Hs Code.:

Synonyms:2-<2-Nitro-3.4.5-trimethoxyphenyl>-3'-methoxy-propiophenon

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Chemical Property of 2-<2-Nitro-3.4.5-trimethoxyphenyl>-3'-methoxy-propiophenon

Chemical Property:

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Technology Process of 2-<2-Nitro-3.4.5-trimethoxyphenyl>-3'-methoxy-propiophenon

There total 7 articles about 2-<2-Nitro-3.4.5-trimethoxyphenyl>-3'-methoxy-propiophenon which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 115001-13-3
2-Nitro-3.4.5-trimethoxybenzyl-3'-methoxybenzoylmalonsaeure-di-tert-butylester

: 109158-32-9
2-<2-Nitro-3.4.5-trimethoxyphenyl>-3'-methoxy-propiophenon

Guidance literature:: With acetic anhydride; toluene-4-sulfonic acid; acetic acid;
DOI:10.1021/ja01500a047

Reference yield:

: 1916-07-0
3,4,5-trimethoxybenzoic acid methyl ester

: 109158-32-9
2-<2-Nitro-3.4.5-trimethoxyphenyl>-3'-methoxy-propiophenon

Guidance literature:: Multi-step reaction with 7 steps

1: Cu(NO₃)2, Ac₂O

2: (alkaline hydrolysis)

3: NaBH₄, BF₃-Et₂O

4: NaH

5: NaH

6: LiNH₂, Fe(NO₃)3

7: Ac₂O, AcOH, TsOH

With sodium tetrahydroborate; lithium amide; boron trifluoride diethyl etherate; acetic anhydride; sodium hydride; copper(II) nitrate; toluene-4-sulfonic acid; acetic acid; ferric nitrate;
DOI:10.1021/ja01500a047

Reference yield:

: 5435-28-9
(3,4,5-trimethoxy-2-nitrophenyl)methanol

: 109158-32-9
2-<2-Nitro-3.4.5-trimethoxyphenyl>-3'-methoxy-propiophenon

Guidance literature:: Multi-step reaction with 4 steps

1: NaH

2: NaH

3: LiNH₂, Fe(NO₃)3

4: Ac₂O, AcOH, TsOH

With lithium amide; acetic anhydride; sodium hydride; toluene-4-sulfonic acid; acetic acid; ferric nitrate;
DOI:10.1021/ja01500a047