3-O-Acetyl-4-<1D-(1N,2,4/3,5,6)-<6-O-acetyl-2,3,4,6-tetrahydroxy-5-C-(hydroxymethyl)-4-O-methylcyclohexyl>amino>-1,6-anhydro-4-desoxy-β-D-glucopyranose

Base Information

Chemical Name:3-O-Acetyl-4-<1D-(1N,2,4/3,5,6)-<6-O-acetyl-2,3,4,6-tetrahydroxy-5-C-(hydroxymethyl)-4-O-methylcyclohexyl>amino>-1,6-anhydro-4-desoxy-β-D-glucopyranose
CAS No.:97119-14-7
Molecular Formula:C₁₈H₂₉NO₁₁
Molecular Weight:435.428
Hs Code.:

Synonyms:3-O-Acetyl-4-<1D-(1N,2,4/3,5,6)-<6-O-acetyl-2,3,4,6-tetrahydroxy-5-C-(hydroxymethyl)-4-O-methylcyclohexyl>amino>-1,6-anhydro-4-desoxy-β-D-glucopyranose

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Chemical Property of 3-O-Acetyl-4-<1D-(1N,2,4/3,5,6)-<6-O-acetyl-2,3,4,6-tetrahydroxy-5-C-(hydroxymethyl)-4-O-methylcyclohexyl>amino>-1,6-anhydro-4-desoxy-β-D-glucopyranose

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Technology Process of 3-O-Acetyl-4-<1D-(1N,2,4/3,5,6)-<6-O-acetyl-2,3,4,6-tetrahydroxy-5-C-(hydroxymethyl)-4-O-methylcyclohexyl>amino>-1,6-anhydro-4-desoxy-β-D-glucopyranose

There total 14 articles about 3-O-Acetyl-4-<1D-(1N,2,4/3,5,6)-<6-O-acetyl-2,3,4,6-tetrahydroxy-5-C-(hydroxymethyl)-4-O-methylcyclohexyl>amino>-1,6-anhydro-4-desoxy-β-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 97119-13-6
3-O-Acetyl-4-<1D-(1N,2,4/3,5,6)-<6-O-acetyl-2,3,7-tri-O-benzyl-2,3,4,6-tetrahydroxy-5-C-(hydroxymethyl)-4-O-methylcyclohexyl>amino>-1,6-anhydro-2-O-benzyl-4-desoxy-β-D-glucopyranose

: 97119-14-7
3-O-Acetyl-4-<1D-(1N,2,4/3,5,6)-<6-O-acetyl-2,3,4,6-tetrahydroxy-5-C-(hydroxymethyl)-4-O-methylcyclohexyl>amino>-1,6-anhydro-4-desoxy-β-D-glucopyranose

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 2h; under 6000.5 Torr;

Reference yield:

: 86845-48-9,86853-28-3
1L-7-O-Acetyl-1-desoxy-1-C-(hydroxymethyl)-2,3:4,5-di-O-isopropyliden-6-O-methyl-myo-inosit

: 97119-14-7
3-O-Acetyl-4-<1D-(1N,2,4/3,5,6)-<6-O-acetyl-2,3,4,6-tetrahydroxy-5-C-(hydroxymethyl)-4-O-methylcyclohexyl>amino>-1,6-anhydro-4-desoxy-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 9 steps

1: 75 percent / 98percent acetic acid / 30 °C

2: 1) 1 N NaOCH₃, 2) NaH / 1) methanol, 1 h, 2) DMF, 2 h, 0 deg C; 5 h, room temp.

3: 91 percent / acetic acid / tetrahydrofuran; H₂O / 60 °C

4: 89 percent / pyridine / CH₂Cl₂ / -40 °C

5: 69 percent / NaN₃ / hexamethylphosphoric acid triamide / 30 °C

6: 86 percent / 4percent NiCl₂-solution, NaBH₄ / ethanol

7: butan-1-ol / 30 h / 110 °C

8: pyridine / 40 °C

9: 94 percent / H₂ / 10percent Pd/C / methanol / 2 h / 6000.5 Torr

With pyridine; sodium tetrahydroborate; sodium azide; hydrogen; sodium methylate; sodium hydride; acetic acid; nickel dichloride; palladium on activated charcoal; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; ethanol; dichloromethane; water; butan-1-ol;

Reference yield:

: 97136-89-5
1L-7-O-Acetyl-1-desoxy-1-C-(hydroxymethyl)-2,3-O-isopropyliden-6-O-methyl-myo-inosit

: 97119-14-7
3-O-Acetyl-4-<1D-(1N,2,4/3,5,6)-<6-O-acetyl-2,3,4,6-tetrahydroxy-5-C-(hydroxymethyl)-4-O-methylcyclohexyl>amino>-1,6-anhydro-4-desoxy-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 8 steps

1: 1) 1 N NaOCH₃, 2) NaH / 1) methanol, 1 h, 2) DMF, 2 h, 0 deg C; 5 h, room temp.

2: 91 percent / acetic acid / tetrahydrofuran; H₂O / 60 °C

3: 89 percent / pyridine / CH₂Cl₂ / -40 °C

4: 69 percent / NaN₃ / hexamethylphosphoric acid triamide / 30 °C

5: 86 percent / 4percent NiCl₂-solution, NaBH₄ / ethanol

6: butan-1-ol / 30 h / 110 °C

7: pyridine / 40 °C

8: 94 percent / H₂ / 10percent Pd/C / methanol / 2 h / 6000.5 Torr

With pyridine; sodium tetrahydroborate; sodium azide; hydrogen; sodium methylate; sodium hydride; acetic acid; nickel dichloride; palladium on activated charcoal; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; ethanol; dichloromethane; water; butan-1-ol;