4-aminophenyl 4'-S-acetyl-2,3,6,2',3',6'-hexa-O-benzoyl-4'-deoxy-4'-thio-β-D-cellobioside

Base Information

Chemical Name:4-aminophenyl 4'-S-acetyl-2,3,6,2',3',6'-hexa-O-benzoyl-4'-deoxy-4'-thio-β-D-cellobioside
CAS No.:934416-62-3
Molecular Formula:C₆₂H₅₃NO₁₇S
Molecular Weight:1116.17
Hs Code.:

Synonyms:4-aminophenyl 4'-S-acetyl-2,3,6,2',3',6'-hexa-O-benzoyl-4'-deoxy-4'-thio-β-D-cellobioside

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Chemical Property of 4-aminophenyl 4'-S-acetyl-2,3,6,2',3',6'-hexa-O-benzoyl-4'-deoxy-4'-thio-β-D-cellobioside

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Technology Process of 4-aminophenyl 4'-S-acetyl-2,3,6,2',3',6'-hexa-O-benzoyl-4'-deoxy-4'-thio-β-D-cellobioside

There total 9 articles about 4-aminophenyl 4'-S-acetyl-2,3,6,2',3',6'-hexa-O-benzoyl-4'-deoxy-4'-thio-β-D-cellobioside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 934416-60-1
4-nitrophenyl 4'-S-acetyl-2,3,6,2',3',6'-hexa-O-benzoyl-4'-deoxy-4'-thio-β-D-cellobioside

: 934416-62-3
4-aminophenyl 4'-S-acetyl-2,3,6,2',3',6'-hexa-O-benzoyl-4'-deoxy-4'-thio-β-D-cellobioside

Guidance literature:: With hydrogen; palladium on activated charcoal; In tetrahydrofuran; methanol; at 20 ℃; for 24h;
DOI:10.1002/anie.200503900

Reference yield:

: 4'-S-acetyl-2,3,6,2',3',6'-hexa-O-benzoyl-4'-deoxy-4'-thio-D-cellobiose

: 934416-62-3
4-aminophenyl 4'-S-acetyl-2,3,6,2',3',6'-hexa-O-benzoyl-4'-deoxy-4'-thio-β-D-cellobioside

Guidance literature:: Multi-step reaction with 3 steps

1: DBU / CH₂Cl₂ / 1.5 h / -40 °C

2: 3.26 g / BF₃*Et₂O / CH₂Cl₂ / 4 h / -40 °C

3: 72 percent / H₂ / Pd/C / tetrahydrofuran; methanol / 24 h / 20 °C

With boron trifluoride diethyl etherate; hydrogen; 1,8-diazabicyclo[5.4.0]undec-7-ene; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1002/anie.200503900

Reference yield:

: C₅₆H₄₇BrO₁₆S

: 934416-62-3
4-aminophenyl 4'-S-acetyl-2,3,6,2',3',6'-hexa-O-benzoyl-4'-deoxy-4'-thio-β-D-cellobioside

Guidance literature:: Multi-step reaction with 4 steps

1: 6.5 g / Ag₂CO₃ / acetone; H₂O / 72 h / 20 °C

2: DBU / CH₂Cl₂ / 1.5 h / -40 °C

3: 3.26 g / BF₃*Et₂O / CH₂Cl₂ / 4 h / -40 °C

4: 72 percent / H₂ / Pd/C / tetrahydrofuran; methanol / 24 h / 20 °C

With boron trifluoride diethyl etherate; hydrogen; 1,8-diazabicyclo[5.4.0]undec-7-ene; silver carbonate; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; water; acetone;
DOI:10.1002/anie.200503900