Heptadecyl-carbamic acid 5-benzyloxymethyl-tetrahydro-furan-2-ylmethyl ester

Base Information

Chemical Name:Heptadecyl-carbamic acid 5-benzyloxymethyl-tetrahydro-furan-2-ylmethyl ester
CAS No.:131729-47-0
Molecular Formula:C₃₁H₅₃NO₄
Molecular Weight:503.766
Hs Code.:

Synonyms:Heptadecyl-carbamic acid 5-benzyloxymethyl-tetrahydro-furan-2-ylmethyl ester

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Chemical Property of Heptadecyl-carbamic acid 5-benzyloxymethyl-tetrahydro-furan-2-ylmethyl ester

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Technology Process of Heptadecyl-carbamic acid 5-benzyloxymethyl-tetrahydro-furan-2-ylmethyl ester

There total 2 articles about Heptadecyl-carbamic acid 5-benzyloxymethyl-tetrahydro-furan-2-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 60656-87-3
benzyloxyacetoaldehyde

: 131729-47-0
Heptadecyl-carbamic acid 5-benzyloxymethyl-tetrahydro-furan-2-ylmethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: diethyl ether / 1 h / Heating

2: 75 percent / m-chloroperbenzoic acid (MCPBA) / CH₂Cl₂ / 24 h / Ambient temperature

3: pyridine / 4 h / 70 °C

With pyridine; 3-chloro-benzenecarboperoxoic acid; In diethyl ether; dichloromethane;
DOI:10.1021/jm00105a058

Reference yield:

: 7418-01-1
heptadecyl isocyanate

: 79494-91-0
5-<(benzyloxy)methyl>tetrahydrofuran-2-methanol

: 131729-47-0
Heptadecyl-carbamic acid 5-benzyloxymethyl-tetrahydro-furan-2-ylmethyl ester

Guidance literature:: With pyridine; at 70 ℃; for 4h;
DOI:10.1021/jm00105a058

Reference yield:

: 131729-47-0
Heptadecyl-carbamic acid 5-benzyloxymethyl-tetrahydro-furan-2-ylmethyl ester

: Carbonic acid 5-heptadecylcarbamoyloxymethyl-tetrahydro-furan-2-ylmethyl ester phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / 5percent Pd/C / CH₂Cl₂; ethanol / 18 h / 5171.5 Torr

2: pyridine / CH₂Cl₂ / 1 h / 0 °C

With pyridine; hydrogen; palladium on activated charcoal; In ethanol; dichloromethane;
DOI:10.1021/jm00105a058