(4R,9aR)-7-azido-9a-methyl-4-phenyl-3,4,9,9a-tetrahydropyrido[2,1-c][1,4]oxazine-1,6-dione

Base Information

Chemical Name:(4R,9aR)-7-azido-9a-methyl-4-phenyl-3,4,9,9a-tetrahydropyrido[2,1-c][1,4]oxazine-1,6-dione
CAS No.:1160107-48-1
Molecular Formula:C₁₅H₁₄N₄O₃
Molecular Weight:298.301
Hs Code.:

Synonyms:(4R,9aR)-7-azido-9a-methyl-4-phenyl-3,4,9,9a-tetrahydropyrido[2,1-c][1,4]oxazine-1,6-dione

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Chemical Property of (4R,9aR)-7-azido-9a-methyl-4-phenyl-3,4,9,9a-tetrahydropyrido[2,1-c][1,4]oxazine-1,6-dione

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Technology Process of (4R,9aR)-7-azido-9a-methyl-4-phenyl-3,4,9,9a-tetrahydropyrido[2,1-c][1,4]oxazine-1,6-dione

There total 1 articles about (4R,9aR)-7-azido-9a-methyl-4-phenyl-3,4,9,9a-tetrahydropyrido[2,1-c][1,4]oxazine-1,6-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 1160107-64-1
(4R,9aR)-9a-methyl-4-phenyl-3,4,9,9a-tetrahydropyrido[2,1-c][1,4]oxazine-1,6-dione

: 1160107-48-1
(4R,9aR)-7-azido-9a-methyl-4-phenyl-3,4,9,9a-tetrahydropyrido[2,1-c][1,4]oxazine-1,6-dione

Guidance literature:: (4R,9aR)-9a-methyl-4-phenyl-3,4,9,9a-tetrahydropyrido[2,1-c][1,4]oxazine-1,6-dione; With bromine; In tetrachloromethane; for 2h; Inert atmosphere; Reflux;

With sodium azide; In N,N-dimethyl-formamide; at 20 - 70 ℃; for 7h;
DOI:10.1021/jo900679c

Reference yield: 69.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 1160107-48-1
(4R,9aR)-7-azido-9a-methyl-4-phenyl-3,4,9,9a-tetrahydropyrido[2,1-c][1,4]oxazine-1,6-dione

: 1160107-50-5
(4R,7R,9aR)-7-(tert-butoxycarbonylamino)-9a-methyl-4-phenylhexahydropyrido[2,1-c][1,4]oxazine-1,6-dione

: 1160107-49-2
(4R,7S,9aR)-7-(tert-butoxycarbonylamino)-9a-methyl-4-phenylhexahydropyrido[2,1-c][1,4]oxazine-1,6-dione

Guidance literature:: With 10% palladium on charcoal; hydrogen; In methanol; for 18h; under 760.051 Torr; diastereoselective reaction;
DOI:10.1021/jo900679c