C₃₃H₃₆O₆

Base Information

• Chemical Name: C₃₃H₃₆O₆
• CAS No.: 194281-34-0
• Molecular Formula: C₃₃H₃₆O₆
• Molecular Weight: 528.645
• Mol file: 194281-34-0.mol

Synonyms:C₃₃H₃₆O₆

Chemical Property of C₃₃H₃₆O₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₃H₃₆O₆

There total 4 articles about C₃₃H₃₆O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

C33H32O6 (194281-36-2) → C33H36O6 (194281-34-0)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethyl acetate; for 16h; under 3750.3 Torr;

DOI:10.1016/S0031-9422(97)00118-0

Reference yield:

3-(4-formylphenoxy)-4-methoxybenzaldehyde (2748-98-3) → C33H36O6 (194281-34-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 87 percent / K₂CO₃, 18-crown-6 / CH₂Cl₂ / 12 h / Heating

2: 82 percent / H₂ / Pd/C / ethyl acetate / 16 h / 3750.3 Torr

With 18-crown-6 ether; hydrogen; potassium carbonate; palladium on activated charcoal; In dichloromethane; ethyl acetate;

DOI:10.1016/S0031-9422(97)00118-0

Reference yield:

isovanillin (621-59-0) → C33H36O6 (194281-34-0)

Guidance literature:

Multi-step reaction with 3 steps

1: 80 percent / K₂CO₃ / dimethylformamide / 4 h / Heating

2: 87 percent / K₂CO₃, 18-crown-6 / CH₂Cl₂ / 12 h / Heating

3: 82 percent / H₂ / Pd/C / ethyl acetate / 16 h / 3750.3 Torr

With 18-crown-6 ether; hydrogen; potassium carbonate; palladium on activated charcoal; In dichloromethane; ethyl acetate; N,N-dimethyl-formamide;

DOI:10.1016/S0031-9422(97)00118-0

upstream raw materials:

C₃₃H₃₂O₆

isovanillin

3-(4-formylphenoxy)-4-methoxybenzaldehyde

4-fluorobenzaldehyde