(+/-)-N-<<<5-(benzyloxy)-3-hydroxypent-1-yl>amino>carbonyl>-3-ethoxy-2-propenamide

Base Information

Chemical Name:(+/-)-N-<<<5-(benzyloxy)-3-hydroxypent-1-yl>amino>carbonyl>-3-ethoxy-2-propenamide
CAS No.:128659-12-1
Molecular Formula:C₁₈H₂₆N₂O₅
Molecular Weight:350.415
Hs Code.:

Synonyms:(+/-)-N-<<<5-(benzyloxy)-3-hydroxypent-1-yl>amino>carbonyl>-3-ethoxy-2-propenamide

Suppliers and Price of (+/-)-N-<<<5-(benzyloxy)-3-hydroxypent-1-yl>amino>carbonyl>-3-ethoxy-2-propenamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)-N-<<<5-(benzyloxy)-3-hydroxypent-1-yl>amino>carbonyl>-3-ethoxy-2-propenamide

Chemical Property:

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Technology Process of (+/-)-N-<<<5-(benzyloxy)-3-hydroxypent-1-yl>amino>carbonyl>-3-ethoxy-2-propenamide

There total 5 articles about (+/-)-N-<<<5-(benzyloxy)-3-hydroxypent-1-yl>amino>carbonyl>-3-ethoxy-2-propenamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 57796-78-8,928778-13-6
(3-ethoxy-acryloyl)isocyanate

: 128631-53-8
(+/-)-1-amino-5-(benzyloxy)pentan-3-ol

: 128659-12-1
(+/-)-N-<<<5-(benzyloxy)-3-hydroxypent-1-yl>amino>carbonyl>-3-ethoxy-2-propenamide

Guidance literature:: In benzene; for 4h; Ambient temperature;
DOI:10.1021/jm00171a022

Reference yield:

: 70388-33-9
4-benzyloxybut-1-ene

: 128659-12-1
(+/-)-N-<<<5-(benzyloxy)-3-hydroxypent-1-yl>amino>carbonyl>-3-ethoxy-2-propenamide

Guidance literature:: Multi-step reaction with 4 steps

1: 87 percent / m-chloroperbenzoic acid / CH₂Cl₂ / Ambient temperature

2: 95 percent / Et₂AlCl / hexane / Ambient temperature

3: 58 percent / LiAlH₄ / diethyl ether / 2 h / Ambient temperature

4: 73 percent / benzene / 4 h / Ambient temperature

With lithium aluminium tetrahydride; diethylaluminium chloride; 3-chloro-benzenecarboperoxoic acid; In diethyl ether; hexane; dichloromethane; benzene;
DOI:10.1021/jm00171a022

Reference yield:

: 128631-52-7
(+/-)-5-(benzyloxy)-3-(trimethylsiloxy)pentanenitrile

: 128659-12-1
(+/-)-N-<<<5-(benzyloxy)-3-hydroxypent-1-yl>amino>carbonyl>-3-ethoxy-2-propenamide

Guidance literature:: Multi-step reaction with 2 steps

1: 58 percent / LiAlH₄ / diethyl ether / 2 h / Ambient temperature

2: 73 percent / benzene / 4 h / Ambient temperature

With lithium aluminium tetrahydride; In diethyl ether; benzene;
DOI:10.1021/jm00171a022