tert-butyl 3-(10H-phenothiazin-10-yl)propyl(4-(2-perfluoroctylethyl)benzyloxy)carbamate

Base Information

• Chemical Name: tert-butyl 3-(10H-phenothiazin-10-yl)propyl(4-(2-perfluoroctylethyl)benzyloxy)carbamate
• CAS No.: 1313585-48-6
• Molecular Formula: C₃₇H₃₃F₁₇N₂O₃S
• Molecular Weight: 908.719

Synonyms:tert-butyl 3-(10H-phenothiazin-10-yl)propyl(4-(2-perfluoroctylethyl)benzyloxy)carbamate

Chemical Property of tert-butyl 3-(10H-phenothiazin-10-yl)propyl(4-(2-perfluoroctylethyl)benzyloxy)carbamate

Chemical Property:

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Technology Process of tert-butyl 3-(10H-phenothiazin-10-yl)propyl(4-(2-perfluoroctylethyl)benzyloxy)carbamate

There total 3 articles about tert-butyl 3-(10H-phenothiazin-10-yl)propyl(4-(2-perfluoroctylethyl)benzyloxy)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

10-(3-chloropropyl)-10H-phenothiazine (5909-59-1) + tert-butyl 4-(2-perfluoroctylethyl)benzyloxycarbamate (1313585-45-3) → tert-butyl 3-(10H-phenothiazin-10-yl)propyl(4-(2-perfluoroctylethyl)benzyloxy)carbamate (1313585-48-6)

Guidance literature:

With caesium carbonate; In acetonitrile; at 45 ℃; for 3h;

DOI:10.1016/j.tet.2011.05.039

Reference yield:

1-(bromomethyl)-4-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)benzene → tert-butyl 3-(10H-phenothiazin-10-yl)propyl(4-(2-perfluoroctylethyl)benzyloxy)carbamate (1313585-48-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / -5 - 20 °C / Inert atmosphere; Darkness

2: caesium carbonate / acetonitrile / 3 h / 45 °C

With caesium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; acetonitrile;

DOI:10.1016/j.tet.2011.05.039

Reference yield:

(4-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)phenyl)methanol (356055-77-1) → tert-butyl 3-(10H-phenothiazin-10-yl)propyl(4-(2-perfluoroctylethyl)benzyloxy)carbamate (1313585-48-6)

Guidance literature:

Multi-step reaction with 3 steps

1: sulfurous dibromide / tetrahydrofuran / 0 - 20 °C / Inert atmosphere; Darkness

2: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / -5 - 20 °C / Inert atmosphere; Darkness

3: caesium carbonate / acetonitrile / 3 h / 45 °C

With sulfurous dibromide; caesium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; acetonitrile;

DOI:10.1016/j.tet.2011.05.039

upstream raw materials:

10-(3-chloropropyl)-10H-phenothiazine

tert-butyl 4-(2-perfluoroctylethyl)benzyloxycarbamate

(4-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)phenyl)methanol

Downstream raw materials:

N-(3-(10H-phenothiazin-10-yl)propyl)-O-(4-(2-perfluoroctyl-ethyl)benzyl)hydroxylamine hydrochloride

C₄₃H₃₇F₁₇N₂O₃S

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