N-acetyl-2-fluoro-4-sulphoaniline triethylamine salt (1:1)

Base Information

• Chemical Name: N-acetyl-2-fluoro-4-sulphoaniline triethylamine salt (1:1)
• CAS No.: 244144-49-8
• Molecular Formula: C₆H₁₅N*C₈H₈FNO₄S
• Molecular Weight: 334.412
• Mol file: 244144-49-8.mol

Synonyms:N-acetyl-2-fluoro-4-sulphoaniline triethylamine salt (1:1)

Chemical Property of N-acetyl-2-fluoro-4-sulphoaniline triethylamine salt (1:1)

Chemical Property:

Purity/Quality:

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Technology Process of N-acetyl-2-fluoro-4-sulphoaniline triethylamine salt (1:1)

There total 1 articles about N-acetyl-2-fluoro-4-sulphoaniline triethylamine salt (1:1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-Fluoroaniline (348-54-9) → N-acetyl-2-fluoro-4-sulphoaniline triethylamine salt (1:1) (244144-49-8)

Guidance literature:

Multi-step reaction with 2 steps

1.1: sulfuric acid / 15 h / 190 °C

1.2: 0.25 h / 0 °C

2.1: 14 h / 0 °C

With sulfuric acid;

Reference yield:

N-acetyl-2-fluoro-4-sulphoaniline triethylamine salt (1:1) (244144-49-8) → 3-fluoro-4-acetamidobenzene sulfonylchloride (349-71-3)

Guidance literature:

N-acetyl-2-fluoro-4-sulphoaniline triethylamine salt (1:1); With trichlorophosphate; at 0 - 20 ℃; for 15.5h;

With water; at 0 ℃; for 0.25h;

upstream raw materials:

2-Fluoroaniline

Downstream raw materials:

3-fluoro-4-acetamidobenzene sulfonylchloride